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At least 19 recordsLinked to original sources
USGS1989

The Uranium-trend dating method: Principles and application for southern California marine terrace deposits

Uranium-trend dating is an open-system method for age estimation of Quaternary sediments, using disequilibrium in the 238U234U230Th decay series. The technique has been applied to alluvium, colluvium, loess, till, and marine sediments. In this study we tested the U-trend dating method on calcareous marine terrace deposits from the Palos Verdes Hills and San Nicolas Island, California. Independent age estimates indicate that terraces in these areas range from ???80 ka to greater than 1.0 Ma. Two low terraces on San Nicolas Island yielded U-trend plots that have a clustered array of points and the ages of these deposits are indeterminate or highly suspect. Middle Pleistocene terraces and one early Pleistocene terrace on San Nicolas Island and all terraces on the Palos Verdes Hills gave reasonably linear U-trend plots and estimated ages that are stratigraphically consistent and in agreement with independent age estimates. We conclude that many marine terrace deposits are suitable for U-trend dating, but U-trend plots must be carefully evaluated and U-trend ages should be consistent with independent geologic control. ?? 1989.

Quaternary International↗
USGS1991

Report of 1st discussion group: The last interglacial in high latitudes of the Northern Hemisphere: Terrestrial and marine evidence

The paleoclimatic informations preserved at some selected sites from high northern latitudes correlative with the last interglacial maximum of Isotopic Substage 5e have been compiled on a hemisphere scale. The mapped compilation reveals much warmer climate conditions on average than present in both terrestrial and marine environments, and indicates a northward shift of subpolar and boreal bioclimatic zones. The data also suggest that temperature and precipitation gradients were significantly different than those of the Holocene, with particularly efficient latitudinal and eastward transport of warm air masses. The paleoenvironmental and paleoclimate trends through the last interglacial sensu lato (Isotopic Stage 5) are more difficult to assess because the chronostratigraphical framework is poorly constrained. Nevertheless, the data suggest important regionalism in the climatostratigraphical trends. In particular, the large amplitude climatic cyclicity that characterizes the last interglacial of Europe is barely observed elsewhere. Moreover, by the end of the last interglacial (Isotopic Substage 5a), conditions slightly cooler than present are recorded in western Europe, while relatively warm conditions, similar to today, apparently prevailed in circumpolar regions adjacent to the North Atlantic despite the onset of ice growth. The last interglacial provides paleosynoptic situations, unlike those of the present, that may contribute to understanding interactions within the environmental system on a hemispheric scale. There is, however, an imperative need for uniformization of data sets and for more accurate chronological control on regional scales.

Quaternary International↗
USGS1991

The last interglaciation in Alaska: Stratigraphy and paleoecology of potential sites

At least 20 localities in Alaska contain deposits that may provide information on the last interglaciation (Oxygen-Isotope Substage 5e). These widely dispersed localities include river bluffs, coastal bluffs and terraces, elevated marine shorelines, lake basins, and artificial excavations. Most of the inferred interglacial deposits contain macrofossils or pollen that are older than the range of radiocarbon dating and commonly indicate climate as warm as or warmer than the present. At a few localities, evidence for deep thaw of permafrost also indicates a warm paleoclimate. At eight localities, the Old Crow tephra occurs at or below organic deposits that may represent Substage 5e. The tephra occurs beneath conspicuous organic deposits at Fairbanks, the Yukon Palisades, and Holitna lowland, and directly above a peat bed at Hogatza Mine. At Birch Creek, Halfway House, Ky-11, and Imuruk Lake, the tephra occurs within a paleosol or organic deposit, but other organic horizons that more likely indicate interglacial conditions occur at higher stratigraphic levels. The varied stratigraphic relations of the Old Crow tephra suggest that it may have been deposited close to the boundary between Isotope Substages 6 and 5, which is dated at about 130 ka in the marine record and between 132 and 140 ka on land. These age relations suggests that the tephra may have been deposited about 135 ?? 5 ka, validating the recent fission-track age determination of 140 ?? 10 ka for this deposit. Six coastal localities contain deposits of probable interglacial age, and these commonly are associated with evidence for eustatic sea levels higher than those of the present. Beach and sublittoral sediments of the Pelukian transgression occur up to 12 m asl along the northwest coast of Alaska, and are correlative with barrier island and lagoonal sediments on the Alaskan Arctic Coastal Plain. Both sets of deposits commonly contain extralimital mollusks and microfauna that indicate marine water slightly warmer than present and suggest that seasonal sea ice did not extend south of Bering Strait during the last interglacial as it does today. Farther south, elevated marine-terrace deposits on Amchitka Island contain marine invertebrates that indicate a climate warmer than at present. Peat horizons in coastal exposure at Goose Bay and coastal terraces at Lituya Bay contain pollen spectra that suggest forests like those of the present day, and spruce macrofossils exposed on Baldwin Peninsula indicate boreal forest more extensive than at present. Sediments from several lakes in northwestern Alaska may contain continuous records of the last interglaciation. A major warm interval, possibly Isotope Substage 5e, has been identified in a core from Squirrel Lake by a peak in Picea pollen that indicates forest extension beyond present limits. Similar pollen records are potentially available from two maars which formed in the Cape Espenberg area more than 125 ka. Terrestrial organic deposits thought to record the last interglaciation occur interstratified with marine and glaciogenic sediments in the Nushagak Lowland of southwest Alaska and on Baldwin Peninsula in Kotzebue Sound. Extensive exposures along the Copper and Nenana Rivers may also contain organic deposits that record the last interglaciation. ?? 1992.

Quaternary International↗
USGS1992

The Pearlette family ash beds in the Great Plains: Finding their identities and their roots in the Yellowstone country

For many years the numerous deposits of so-called 'Pearlette volcanic ash' in the Great Plains region of the United States were considered to be the remnants of the same volcanic event, and were used as a time-stratigraphic marker of probable Middle Pleistocene age. Although a few early workers had suggested that more than one air-fall event might be represented among the Pearlette occurrences, it was not until the latter half of the present century, after identification of volcanic ash beds by detailed chemical and mineralogical methods had been developed, that it could be established that the 'Pearlette family' of volcanic ashes included three ash beds of subtly differing characteristics. Development of isotopic methods of age determination has established that the ages of the three are significantly different (2.09, 1.29, and 0.60 Ma). The area of distribution of the Pearlette family ash beds was found to include not only the Great Plains, but also to extend across the Rocky Mountain and the Basin and Range provinces to the Pacific Ocean. The search for the sources of these three similar appearing ash beds, facilitated greatly by information gained from concurrent mapping projects underway in areas of major Late Cenozoic volcanic activity in western United States, ultimately led to the sites of the caldera-forming eruptions in the Yellowstone National Park region. ?? 1992.

Quaternary International↗
USGS1992

Fluvial deposits of Yellowstone tephras: Implications for late Cenozoic history of the Bighorn basin area, Wyoming and Montana

Several deposits of tephra derived from eruptions in Yellowstone National Park occur in the northern Bighorn basin area of Wyoming and Montana. These tephra deposits are mixed and interbedded with fluvial gravel and sand deposited by several different rivers. The fluvial tephra deposits are used to calculate stream incision rates, to provide insight into drainage histories and Quaternary tectonics, to infer the timing of alluvial erosion-deposition cycles, and to calibrate rates of soil development. ?? 1992.

Quaternary International↗
USGS1992

Net Late Holocene emergence despite earthquake-induced submergence, south-central Chile

Intertidal deposits show net Late Holocene emergence at three sites along the Pacific coast near Maulli??n and Carelmapu, Chile (latitude 41.6-41.7??S.). The maximum amount of net emergence is ca. 1 m in the past 1500 years and ca. 2 1 2 m in the past 4000 years. Emergence probably would have prevailed at a fourth site near Maulli??n were the site not underlain by easily compacted deposits; this site shows slight (< 1 m) net submergence in the past 3000 years. Despite net emergence, all four sites underwent 1-2 m of submergence from tectonic subsidence during a magnitude-9.5 earthquake in 1960, and two of the sites show evidence for earlier submergence events of Late Holocene age. The net emergence is probably due to some combination of cyclic uplift from elastic strain accumulation between earthquakes and monotonic uplift from postglacial loading of the Pacific Ocean floor. The small amount of the net emergence shows that neotectonics has had little net impact on Holocene relative sea level in part of the focal region of the largest earthquake recorded by seismograph. ?? 1992.

Quaternary International↗
USGS1993

Deposition of the late Wisconsin Johnstown moraine, south-central Wisconsin

The Johnstown moraine is made up of three different materials. The lower part of the sequence consists of closely spaced bodies of boulder gravel, which are cylindrical and plunge upglacier several degrees. They are interpreted to be esker bodies. They grade distally into proglacial outwash fans. The esker bodies are overlain by sandy till, some of which is uniform and some of which has colour layers. The colour layers are a few millimetres to a metre thick, drape over the eskers and dip upglacier several degrees. Both the uniform and layered till have pebbles plunging upglacier several degrees steeper than the dip of the layers. Both the uniform and layered till are interpreted to have been deposited subglacially, probably both by melting out and by lodgement. The till is overlain by a thin layer of boulder gravel interpreted to be washed supraglacial sediment. ?? 1993.

Quaternary International↗
USGS1994

Miocene and Pliocene lacustrine and fluvial sequences, Upper Ramparts and Canyon village, Porcupine river, east-central Alaska

Cenozoic strata exposed along the Porcupine River between the Upper Ramparts and Canyon Village, Alaska, can be divided into five unconformity-bounded units (sequences) which are: lower and middle Miocene unit A, the white sandy fluvial sequence with peat beds; middle Miocene unit B, the basalt sequence-part B1 is basalt, and part B2 is organic-rich sedimentary beds; upper Miocene unit C, mudrock-dominated lake sequence; late Miocene or Pliocene to Pleistocene unit D, terrace gravels, detrital organic matter and associated sediments, and Holocene unit E, mixed sand and gravel-rich sediment and other sedimentary material including peat and eolian silt. The sequence (unit A) of lower and middle Miocene fluvial deposits formed in streams and on flood plains, just before the inception of local volanism. Fossil pollen from unit A suggests conifer-dominated regional forests and cool temperate climates. Peat beds and lake deposits from unit B contain pollen that indicates a warmer temperate climate coinciding with the middle Miocene thermal maximum. The lake deposits (unit C) downstream from the basalts accumulated in a small basin which resulted from a hydrologic system that was dammed in the late Miocene but breached soon thereafter. The lower part of the terrace gravels (unit D) expresses breaching of the dammed hydrologic system (of unit C). The Porcupine River became a major tributary of the Yukon River in late Pleistocene time when Laurentide ice blocked drainage from the Yukon interior basins causing meltwater to spill over the low divide separating it from the Porcupine River drainage initiating erosion and capture of the Yukon interior basins. ?? 1994.

Quaternary International↗
USGS1994

40Ar 39Ar age constraints on neogene sedimentary beds, Upper Ramparts, half-way Pillar and Canyon village sites, Porcupine river, east-central Alaska

40 Ar/ 39 Ar ages of volcanic rocks are used to provide numerical constraints on the age of middle and upper Miocene sedimentary strata collected along the Porcupine River. Intercalated sedimentary rocks north of latitude 67°10′N in the Porcupine terrane of east-central Alaska contain a rich record of plant fossils. The fossils are valuable indicators of this interior region's paleoclimate during the time of their deposition. Integration of the 40 Ar/ 39 Ar 40 Ar 39 Ar "> results with paleomagnetic and sedimentological data allows for refinements in estimating the timing of deposition and duration of selected sedimentary intervals. 40 Ar 39 Ar "> 40Ar39Ar plateau age spectra, from whole rock basalt samples, collected along the Upper Ramparts and near Half-way Pillar on the Porcupine River, range from 15.7 ± 0.1 Ma at site 90-6 to 14.4 ± 0.1 Ma at site 90-2. With exception of the youngest basalt flow at site 90-2, all of the samples are of reversed magnetic polarity, and all 40 Ar/ 39 Ar age spectrum results are consistent with the deposition of the entire stratigraphic section during a single interval of reversed magnetic polarity. The youngest flow at site 90-2 was emplaced during an interval of normal polarity. With age, paleomagnetic and sedimentological data, the ages of the Middle Miocene sedimentary rocks between the basalt flows at sites 90-1 and 90-2 can be assigned to an interval within the limits of analytical precision of 15.2 ± 0.1 Ma; thus, the sediments were deposited during the peak of the Middle Miocene thermal maximum. Sediments in the upper parts of sites 90-1 and 90-2 were probably deposited during cooling from the Middle Miocene thermal maximum. 40 Ar/ 39 Ar results of plagioclase and biotite from a single tephra, collected at sites 90-7 and 90-8 along the Canyon Village section of the Porcupine River, indicate an age of 6.57 ± 0.02 Ma for its time of eruption and deposition. These results, together with sedimentological and paleomagnetic data, suggest that all of the Upper Miocene lacustrine sedimentary rocks at these sites were deposited during a single interval of reversed magnetic polarity and may represent a duration of only about 40,000 years. The age of this tephra corresponds with a late late Miocene warm climatic interval. The results from the Upper Ramparts and Half-way Pillar sites are used to estimate a minimum interval of continental flood basalt activity of 1.1–1.5 million years, and to set limits for the timing and duration of Tertiary extensional tectonic activity in the Porcupine terrane. Our data indicate that the oroclinal flexure that formed before the deposition of the basalts at the eastern end of the Brooks Range was created prior to 15.7 ± 0.1 Ma.

Alaska↗
USGS1997

Preliminary results of the first scientific Drilling on Lake Baikal, Buguldeika site, southeastern Siberia

The Baikal Drilling Project (BDP) is a multinational effort to investigate the paleoclimatic history and tectonic evolution of the Baikal sedimentary basin during the Late Neogene. In March 1993 the Baikal drilling system was successfuly deployed from a barge frozen into position over a topographic high, termed the Buguldeika saddle, in the southern basin of Lake Baikal. The BDP-93 scientific team, made up of Russian, American and Japanese scientists, successfully recovered the first long (>100 m) hydraulic piston cores from two holes in 354 m of water. High quality cores of 98 m (Hole 1) and 102 m (Hole 2), representing sedimentation over the last 500,000 years, were collected in 78 mm diameter plastic liners with an average recovery of 72% and 90%, respectively. Magnetic susceptibility logging reveals an excellent hole-to-hole correlation. In this report the scientific team describes the preliminary analytical results from BDP-93 hole 1 cores. Radiocarbon dating by accelerator mass spectrometry provides an accurate chronology for the upper portion of Hole 1. Detailed lithologic characteristics, rock magnetic properties and inorganic element distributions show a significant change to the depositional environment occuring at 50 m subbottom depth, approximately 250,000 BP. This change may be due to uplift and rotation of the horst block in the Buguldeika saddle. The sedimentary section above 50 m is pelitic with varve-like laminae, whereas the section below 50 m contains a high proportion of sand and gravel horizons often organized into turbidite sequences. Accordingly, high resolution seismic records reveal a change in sonic velocity at this depth. It is inferred that sedimentation prior to 250 ka BP was from the west via the Buguldeika river system. After 250 ka BP the Buguldeika saddle reflects an increase in hemipelagic sediments admixed with fine-grained material from the Selenga River drainage basin, east of Lake Baikal. Variations in the spore-pollen assemblage, diatoms, biogenic silica content, rock magnetic properties, clay mineralogy and organic carbon in the upper 50 m of BDP-93-1 reveal a detailed record of climate change over approximately the last 250,000 years. These variables alternate in a pattern characteristic of glacial/interglacial climatic fluctuations. The present age model suggests that the climate signal recorded in Lake Baikal sediments is similar to Late Quaternary signals recorded in Chinese loess sections and in marine sediments.

Siberia↗
USGS2006

Late Quaternary landscape evolution in the Kunlun Mountains and Qaidam Basin, Northern Tibet: A framework for examining the links between glaciation, lake level changes and alluvial fan formation

The Qaidam Basin in Northern Tibet is one of the largest hyper-arid intermontane basins on Earth. Alluvial fans, pediment surfaces, shorelines and a thick succession of sediments within the basin, coupled with moraines and associated landforms in the adjacent high mountain catchments of the Kunlun Mountains, record a complex history of Late Quaternary paleoenvironmental change and landscape evolution. The region provides an ideal natural laboratory to examine the interaction between tectonics and climate within a continent-continent collision zone, and to quantify rates of landscape evolution as controlled by climate and the associated glacial and hydrological changes in hyper-arid and adjacent high-altitude environments. Geomorphic mapping, analysis of landforms and sediments, and terrestrial cosmogenic radionuclide surface exposure and optically stimulated luminescence dating serve to define the timing of formation of Late Quaternary landforms along the southern and northwestern margins of the Qaidam Basin, and in the Burhan Budai Shan of the Kunlun Mountains adjacent to the basin on the south. These dates provide a framework that suggests links between climatic amelioration, deglaciation, lake desiccation and alluvial fan evolution. At least three glacial advances are defined in the Burham Budai Shan of the Kunlun Mountains. On the northern side of this range these occurred in the penultimate glacial cycle or early in the last glacial cycle, during the Last Glacial Maximum (LGM)/Lateglacial and during the Holocene. On the south side of the range, advances occurred during the penultimate glacial cycle, MIS-3, and possibly the LGM, Lateglacial or Holocene. Several distinct phases of alluvial fan sedimentation are likewise defined. Alluvial fans formed on the southern side of the Kunlun Mountains prior to 200 ka. Ice-contact alluvial fans formed during the penultimate glacial and during MIS-3. Extensive incised alluvial fans that form the main valley fills north of the Burham Budai and extend into the Qaidam Basin are dated to ???30 ka. These ages suggest that there was a period of alluvial fan aggradation and valley filling that persisted until desiccation of the large lakes in the Qaidam Basin post ???30 ka led to base level lowering and active incision of streams into the valley fills. The continued Lateglacial and Holocene desiccation likely led to further degradation of the valley fills. Ice wedge casts in the Qaidam Basin date to ???15 ka, indicating significant Lateglacial climatic amelioration, while Holocene loess deposits north of the Burham Bdudai suggest that aridity has increased in the region since the early Holocene. From these observations, we infer that the major landscape changes within high glaciated mountains and their adjacent hyper-arid intermontane basins, such as the Kunlun Mountains and Qaidam Basin, occur rapidly over millennial timescales during periods of climatic instability. ?? 2006 Elsevier Ltd and INQUA.

Quaternary International↗
USGS2007

Mammoth (Mammuthus sp.) excavation on a college campus in Western Illinois, USA

The discovery of the remains of a mammoth, Mammuthus sp., on the Principia College campus in Elsah, Illinois, has allowed for careful excavation by students over several years. The mammoth is relatively well preserved in late Wisconsin Peoria Silt on the top of the bluffs of the Mississippi River. The mammoth was buried by loess, perhaps as a result of persistent dust storms, approximately 17 500 14C years ago. This age estimate is based on the mammoth's stratigraphic position within the Peoria Silt and is loosely supported by an AMS radiocarbon age on poorly preserved collagen from tooth dentine (???17 810??4300 14C years [CAMS #104172]). Over one hundred bones or bone pieces have been excavated to-date. The skull, containing the tusks and maxillary teeth, is complete and in close proximity to associated postcranial remains, indicating that the mammoth died where it was found. The size and characteristics of skeletal elements have allowed us to determine that this was a mature male of about 41 years of age. Taxonomic attribution-either to Mammuthus primigenius or Mammuthus jeffersonii-is pending, based on the outcome of thorough analysis once the skull with dentition has been prepared from enclosing matrix. ?? 2006 Elsevier Ltd and INQUA.

Quaternary International↗
USGS2008

Stratigraphic and compositional complexities of the late Quaternary Lethe tephra in South-central Alaska

Recently discovered Lethe tephra has been proposed as a latest Pleistocene marker bed in Bristol Bay lowland NE to the Cook Inlet region, Alaska, on the basis of correlations involving a single "Lethe average" glass composition. Type deposits in the Valley of Ten Thousand Smokes, however, are chemically heterogeneous-individual lapilli as well as aggregate ash deposits have glass compositions that range from the average mode to much higher SiO2 and K2O. Moreover, a lake-sediment core from the Cook Inlet region contains one ash deposit similar to "Lethe average" and other, closely underlying deposits that resemble a mixture of the average mode and high-Si high-K mode of proximal deposits. Synthesis of previously published radiocarbon ages indicates a major eruption mainly of "Lethe average" mode about 13,000 14C yr BP. As many as six deposits in the Cook Inlet region-five chiefly "Lethe average" mode-range from about 13,000 to 15-16,000 14C yr BP, and an early Holocene deposit in the Bristol Bay lowland extends the minimum age range of Lethe tephra throughout this region to 8000 14C yr BP. Because of the appearance of "Lethe average" composition in multiple deposits spanning thousands of years, we urge caution when using a Lethe-like composition as a basis for inferring a latest Pleistocene age of a tephra deposit in south-central Alaska. Linear variation plots suggest that magma mixing caused the Lethe heterogeneity; multiple magmas were involved as well in other large pyroclastic eruptions such as Katmai (Alaska) and Rotorua (New Zealand). Lethe is an example of a heterogeneous tephra that may be better compared with other tephras by use of plots of individual analytical points rather than by calculating similarity coefficients based on edited data. ?? 2006 Elsevier Ltd and INQUA.

Quaternary International↗
USGS2007

Holocene sea level and climate change in the Black Sea: Multiple marine incursions related to freshwater discharge events

Repeated marine invasions of the Black Sea during the Holocene have been inferred by many eastern scientists as resulting from episodes of marine inflow from the Mediterranean beneath a brackish outflow from the Black Sea. We support this scenario but a fundamental question remains: What caused the repeated marine invasions? We offer an hypothesis for the repeated marine invasions of the Black Sea based on: (1) the overall similarity of sea-level curves from both tectonically quiescent and active margins of the Black Sea and their similarity to a sequence stratigraphic record from the US mid-Atlantic coast. The similarity of the records from two widely-separated regions suggests their common response to documented Holocene climate ocean-atmosphere reorganizations (coolings); (2) the fact that in the modern Black Sea, freshwater runoff from surrounding rivers dominates over evaporation, so that excess runoff might have temporarily raised Black Sea level (although the Black Sea would have remained brackish). Following the initial invasion of the Black Sea by marine Mediterranean waters (through the Marmara Sea) in the early Holocene, repeated marine incursions were modulated, or perhaps even caused, by freshwater discharge to the Black Sea. Climatic amelioration (warming) following each documented ocean-atmosphere reorganization during the Holocene likely shifted precipitation patterns in the surrounding region and caused mountain glaciers to retreat, increasing freshwater runoff above modern values and temporarily contributing to an increase of Black Sea level. Freshwater-to-brackish water discharges into the Black Sea initially slowed marine inflow but upon mixing of runoff with more marine waters beneath them and their eventual exit through the Bosphorus, marine inflow increased again, accounting for the repeated marine invasions. The magnitude of the hydrologic and sea-level fluctuations became increasingly attenuated through the Holocene, as reflected by Black Sea level curves. ?? 2006 Elsevier Ltd and INQUA.

Quaternary International↗
USGS2007

Late Quaternary stratigraphy and luminescence geochronology of the northeastern Mojave Desert

The chronology of the Holocene and late Pleistocene deposits of the northeastern Mojave Desert have been largely obtained using radiocarbon ages. Our study refines and extends this framework using optically stimulated luminescence (OSL) to date deposits from Valjean Valley, Silurian Lake Playa, Red Pass, and California Valley. Of particular interest are eolian fine silts incorporated in ground-water discharge (GWD) deposits bracketed at 185-140 and 20-50 ka. Alluvial fan deposits proved amenable for OSL by dating both eolian sand lenses and reworked eolian sand in a matrix of gravel that occurs within the fan stratigraphy. Lacustrine sand in spits and bars also yielded acceptable OSL ages. These OSL ages fill gaps in the geochronology of desert deposits, which can provide data relevant to understanding the responses of several depositional systems to regional changes in climate. This study identifies the most promising deposits for future luminescence dating and suggests that for several regions of the Mojave Desert, sediments from previously undated landforms can be more accurately placed within correct geologic map units.

Quaternary International↗
USGS2007

230Th-U dating of surficial deposits using the ion microprobe (SHRIMP-RG): A microstratigraphic perspective

We used the sensitive high-resolution ion microprobe reverse-geometry (SHRIMP-RG) to date pedogenic opal using the 230 Th–U system. Due to the high-spatial resolution of an ion microprobe (typically 30 μm), regions of pure opal within a sample can be targeted and detrital material can be avoided. In addition, because the technique is non-destructive, the sample can be preserved for other types of analyses including electron microprobe or other stable isotope or trace element ion microprobe measurements. The technique is limited to material with U concentrations greater than ∼50 ppm. However, the high spatial resolution, small sample requirements, and the ability to avoid detrital material make this technique a suitable technique for dating many Pleistocene deposits formed in semi-arid environments. To determine the versatility of the method, samples from several different deposits were analyzed, including silica-rich pebble coatings from pedogenic carbonate horizons, a siliceous sinter deposit, and opaline silica deposited as a spring mound. U concentrations for 30-μm-diameter spots ranged from 50 to 1000 ppm in these types of materials. The 230 Th/ 232 Th activity ratios also ranged from ∼100 to 10 6 , eliminating the need for detrital Th corrections that reduce the precision of traditional U-Th ages for many milligram- and larger-sized samples. In pedogenic material, layers of high-U opal (ca. 500 ppm) are commonly juxtaposed next to layers of calcite with much lower U concentrations (1–2 ppm). If these types of samples are not analyzed using a technique with the appropriate spatial resolution, the ages may be strongly biased towards the age of the opal. Comparison with standard TIMS (Thermal Ionization Mass Spectrometry) measurements from separate microdrilled samples suggests that although the analytical precision of the ion microprobe (SHRIMP-RG) measurements is less than TIMS, the high spatial resolution results in better accuracy in the age determination for finely layered or complex deposits. The ion microprobe approach also may be useful for pre-screening samples to determine the age and degree of post-depositional alteration, analyzing finely layered samples or samples with complex growth histories, and obtaining simultaneous measurements of trace elements.

Quaternary International↗
USGS2008

Determining an age for the Inararo Tuff eruption of Mt. Pinatubo, based on correlation with a distal ash layer in core MD97-2142, South China Sea

The largest known eruption of Mt. Pinatubo in the late Quaternary was the Inararo Tuff Formation (ITF) eruption, roughly estimated as five times larger than the 1991 eruption. The precise age of the ITF eruption has been uncertain. Here, a correlative of the ITF eruption, Layer D, is identified in marine sediments, and an age obtained. Tephras were identified in core MD97-2142 of Leg II of the IMAGES III cruise in northern offshore of Palawan, southeastern South China Sea (12??41.33???N, 119??27.90???E). On the basis of the geochemical and isotopic fingerprints, Layer D can be correlated with the ITF eruption of the modern Pinatubo-eruption sequence. By means of the MD97-2142 SPECMAP chronology, Layer D was dated at around 81??2 ka. This estimated age of the ITF eruption and tephra Layer D coincides with an anomalously high SO4-2 spike occurring within the 5 millennia from 79 to 84 ka in the GISP2 ice core record. ?? 2007.

Quaternary International↗