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Quaternary geochronology using combined U-Pb and U-series methods: The opal perspective
No abstract available.
206Pb-230Th-234U-238U and 207Pb-235U geochronology of Quaternary opal, Yucca Mountain, Nevada
U–Th–Pb isotopic systems have been studied in submillimeter-thick outermost layers of Quaternary opal occurring in calcite–silica fracture and cavity coatings within Tertiary tuffs at Yucca Mountain, Nevada, USA. These coatings preserve a record of paleohydrologic conditions at this site, which is being evaluated as a potential high-level nuclear waste repository. The opal precipitated from groundwater is variably enriched in 234 U (measured 234 U/ 238 U activity ratio 1.124–6.179) and has high U (30–313 ppm), low Th (0.008–3.7 ppm), and low common Pb concentrations (measured 206 Pb/ 204 Pb up to 11,370). It has been demonstrated that the laboratory acid treatment used in this study to clean sample surfaces and to remove adherent calcite, did not disturb U–Th–Pb isotopic systems in opal. The opal ages calculated from 206 Pb∗/ 238 U and 207 Pb∗/ 235 U ratios display strong reverse discordance because of excess radiogenic 206 Pb∗ derived from the elevated initial 234 U. The data are best interpreted using projections of a new four-dimensional concordia diagram defined by 206 Pb∗/ 238 U, 207 Pb∗/ 235 U, 234 U/ 238 U activity , and 230 Th/ 238 U activity . Ages and initial 234 U/ 238 U activity ratios have been calculated using different projections of this diagram and tested for concordance. The data are discordant, that is observed 207 Pb∗/ 235 U ages of 170 ± 32 (2σ) to 1772 ± 40 ka are systematically older than 230 Th/U ages of 34.1 ± 0.6 to 452 ± 32 ka. The age discordance is not a result of migration of uranium and its decay products under the open system conditions, but a consequence of noninstantaneous growth of opal. Combined U–Pb and 230 Th/U ages support the model of slow mineral deposition at the rates of millimeters per million years resulting in layering on a scale too fine for mechanical sampling. In this case, U–Pb ages provide more accurate estimates of the average age for mixed multiage samples than 230 Th/U ages, because ages based on shorter-lived isotopes are nonlinearly biased by younger mineral additions. Use of the combined U–Th–Pb technique to date Yucca Mountain Quaternary opals significantly extends the age range beyond that of the 230 Th/U dating method and shows that selected fracture pathways in the unsaturated zone felsic tuffs of Yucca Mountain have been active throughout the Quaternary.
Surficial geology and Quaternary fault map of the Las Vegas Valley, Clark County, Nevada
The Surficial Geology and Quaternary Fault Map of the Las Vegas Valley, Clark County, Nevada is a 1:50,000-scale compilation of published 1:24,000-scale geologic maps integrated with new field and desktop mapping. This geologic map compilation and GIS database are part of a broader study on the Quaternary faults in the Las Vegas Valley, the results of which are summarized in this report. The map compilation utilized a variety of digital base maps to evaluate the characteristics of surficial deposits and Quaternary fault scarps including lidar data in undeveloped parts of the valley and orthorectified historical aerial photos in the urbanized center of the valley. The map distinguishes twenty surficial map units including alluvial-fan and ephemeral-wash deposits, groundwater discharge deposits of the Las Vegas Formation, and alluvium deposits of Las Vegas Wash. Quaternary faults include the Quaternary Las Vegas Valley fault system in the center of the valley and the Frenchman Mountain fault system along the eastern margin. All Quaternary fault traces in the valley were evaluated, and the previously published fault mapping was modified as needed. The new mapping and uniform correlation of surficial deposits displaced by Quaternary faults yields a consistent valley-wide characterization of the recency of fault activity. The map and GIS database include a Quaternary geochronology compilation of 119 previously published surficial deposit ages of various types, 35 new luminescence ages, and 3 new radiocarbon ages. The new age data further bracket the ages of the Las Vegas basin Quaternary stratigraphy and provide new constraints on the timing of Quaternary fault activity.
Proceedings of Conference on Status of Geologic Research and Mapping, Death Valley National Park
Welcome to this conference on the “Status of Geologic Research and Mapping in Death Valley National Park.” We organized this conference in an effort to foster communication and increase awareness among parties conducting geologic research in and around the park. Additionally, we hope to assess the status of geologic mapping efforts within the park boundaries in an effort to provide a framework for future discussions regarding the impact and merits of the development of a park-wide geologic map. The topics presented at this meeting reflect the breadth of recent and ongoing geologic research in and near Death Valley National Park. Sessions include (1) regional structure, tectonics, and bedrock geology; (2) Neogene basin stratigraphy, geophysics, and hydrology; (3) posters on mapping in the Death Valley region and topical ones on Death Valley National Park; (4) imagery, Quaternary stratigraphy and geomorphology, and Quaternary geochronology; and (5) paleoclimate and active tectonics. On a one-day field trip to Death Valley, we will visit areas of “type locality” status as well as areas of new research.
Late Quaternary stratigraphy and geochronology of the western Killpecker Dunes, Wyoming, USA
New stratigraphic and geochronologic data from the Killpecker Dunes in southwestern Wyoming facilitate a more precise understanding of the dune field's history. Prior investigations suggested that evidence for late Pleistocene eolian activity in the dune field was lacking. However, luminescence ages from eolian sand of ???15,000 yr, as well as Folsom (12,950-11,950 cal yr B.P.) and Agate Basin (12,600-10,700 cal yr) artifacts overlying eolian sand, indicate the dune field existed at least during the latest Pleistocene, with initial eolian sedimentation probably occurring under a dry periglacial climate. The period between ???13,000 and 8900 cal yr B.P. was characterized by relatively slow eolian sedimentation concomitant with soil formation. Erosion occurred between ???8182 and 6600 cal yr B.P. on the upwind region of the dune field, followed by relative stability and soil formation between ???5900 and 2700 cal yr B.P. The first of at least two latest Holocene episodes of eolian sedimentation occurred between ???2000 and 1500 yr, followed by a brief (???500 yr) episode of soil formation; a second episode of sedimentation, occurring by at least ???700 yr, may coincide with a hypothesized Medieval warm period. Recent stabilization of the western Killpecker Dunes likely occurred during the Little Ice Age (???350-100 yr B.P.). The eolian chronology of the western Killpecker Dunes correlates reasonably well with those of other major dune fields in the Wyoming Basin, suggesting that dune field reactivation resulted primarily due to departures toward aridity during the late Quaternary. Similar to dune fields on the central Great Plains, dune fields in the Wyoming Basin have been active under a periglacial climate during the late Pleistocene, as well as under near-modern conditions during the latest Holocene. ?? 2003 University of Washington. All rights reserved.
Revisiting the geochronology of late Quaternary marine terraces and uplift rates in coastal Santa Barbara County, California, USA
In several early studies, central California marine terraces between Santa Barbara and Point Conception were interpreted to record sea-level high stands of the last interglacial complex, ∼80 ka to ∼120 ka (marine isotope stage [MIS] 5). These ages and their elevations (∼20 m to ∼45 m) indicate modest rates of tectonic uplift, similar to those from other localities in southern and central California. A recent study, using a combination of luminescence and radiocarbon dating, has challenged the older age interpretations, implying much younger terrace ages, between ∼40 ka and ∼55 ka (MIS 3). From these new ages and a considerably lower sea level during MIS 3, much higher rates of tectonic uplift are inferred. In the present study, new uranium-series ages of terrace corals and amino acid age estimates of terrace mollusks were determined to test these competing interpretations. With the exception of a low-elevation terrace in Isla Vista (near Santa Barbara) that dates to MIS 3, terraces farther west are interpreted to date to MIS 5 and imply tectonic uplift rates of 0.20–0.34 m/kyr. A compilation of data for the region yields a decreasing rate of late Quaternary uplift from east, near Ventura, to west, near Point Conception. This trend is interpreted to reflect a decreasing influence of the processes of compression and crustal shortening south of the Big Bend in the San Andreas fault.
Reconciliation of geochronology and paleozoogeography for Quaternary marine terraces, San Luis Obispo Bay area, California, USA
In the San Luis Obispo Bay area of central California, interpretations of marine terrace ages have been hampered by inconsistent results from geochronological indicators (U-series ages of corals and correlations using amino acid racemization of mollusks) and seemingly contradictory paleozoogeographic aspects of fossil faunal assemblages. New U-series ages of corals, amino acid data from mollusks, and detailed analyses of fossil mollusk assemblages are presented that reconcile many of the apparently discordant results from previous studies. The two lowest-elevation terraces are Q1 (lower) and Q2 (upper); both are thought to date from high-sea stands of marine isotope stage (MIS) 5, the last interglacial complex. A combination of U-series dating and amino acid racemization results indicates that the Q1 terrace probably dates to the ∼80 ka high-sea stand of MIS 5a. U-series analyses of corals from the Q2 terrace show open-system histories, but consideration of two alternative open-system histories indicates that this terrace likely hosts corals dating to the high-sea stands of MIS 5c (∼105–95 ka) and MIS 5e (∼130–115 ka). Amino acid ratios in the fossil bivalve Leukoma staminea (Conrad, 1837) support the age differences between the two terraces and the open-system models suggested by the U-series data. Alkenone studies along much of the coast of California have shown that sea surface temperatures (SSTs) of the eastern Pacific Ocean were warmer than present during MIS 5e. During MIS 5c, on the other hand, SSTs were either similar to the present or cooler, but in either case, much cooler than during MIS 5e. The paleozoogeographic aspects of the molluscan faunas from the Q2 terrace support an interpretation that these deposits contain a mixture of fossils from both the MIS 5c and 5e high-sea stands. Fossils from the Q2 terrace include southern or southward-ranging species (likely dating to MIS 5e) and northern or northward-ranging species (likely dating to MIS 5c). A mixture of MIS 5e and MIS 5c fossils on the Q2 terrace is consistent with similar data reported for other localities in California. This phenomenon is explained by glacial isostatic adjustment (GIA) processes, which brought about a higher-than-present sea level during MIS 5c. GIA processes, combined with a low uplift rate, allowed mixing of MIS 5e fossils during the MIS 5c high-sea stand through capture of an MIS 5e terrace that had experienced minimal uplift in ∼20,000 years. Terrace reoccupation and fossil mixing such as that in the San Luis Obispo Bay area can be expected along any part of the Pacific Coast of North America that was affected by GIA processes and where uplift rates are low.
Late Quaternary stratigraphy and luminescence geochronology of the northeastern Mojave Desert
The chronology of the Holocene and late Pleistocene deposits of the northeastern Mojave Desert have been largely obtained using radiocarbon ages. Our study refines and extends this framework using optically stimulated luminescence (OSL) to date deposits from Valjean Valley, Silurian Lake Playa, Red Pass, and California Valley. Of particular interest are eolian fine silts incorporated in ground-water discharge (GWD) deposits bracketed at 185-140 and 20-50 ka. Alluvial fan deposits proved amenable for OSL by dating both eolian sand lenses and reworked eolian sand in a matrix of gravel that occurs within the fan stratigraphy. Lacustrine sand in spits and bars also yielded acceptable OSL ages. These OSL ages fill gaps in the geochronology of desert deposits, which can provide data relevant to understanding the responses of several depositional systems to regional changes in climate. This study identifies the most promising deposits for future luminescence dating and suggests that for several regions of the Mojave Desert, sediments from previously undated landforms can be more accurately placed within correct geologic map units.
Zircon geochronology and geochemistry of Quaternary rhyolite domes of the Coso volcanic field, Inyo County, California
The Quaternary Coso volcanic field (CVF) is a compositionally bimodal volcanic field located within a releasing bend along the eastern range-front Sierra Nevada fault zone in California's southern Owens Valley. The erupted products of CVF silicic magmatism since ~1 Ma comprise 38 high-silica rhyolite domes, with the volumetric majority (~99%) of rhyolite emplaced within the past ~300 ka. The CVF hosts an economically important geothermal field driven by heat associated with a shallow (~5 km) igneous intrusion. The CVF is potentially an immature analog to the nearby Long Valley system, which culminated in generation and eruption of the voluminous and widespread Bishop Tuff. As such, the CVF represents a considerable volcanic hazard, making a detailed understanding of the eruptive history and pre-eruptive conditions of the system critically important. We present uranium-series isochron dates from zircon ± allanite crystal surfaces and zircon trace element geochemical data on the youngest 17 rhyolite domes at Coso, which represent ~60% (by volume) of the silicic magma erupted by the system. These data suggest: (1) a shorter emplacement duration than previously recognized for these domes, with a duration of 20 ± 5 ka; (2) 4 shorter-duration eruption pulses within this interval, all of which occur during the marine isotope stage (MIS) 5 interglacial period; (3) an uptick in the volume of CVF magma erupted between ~200 ka and ~ 78 ka relative to that emplaced over the lifetime of the system; (4) near-coeval eruption of geochemically distinct magma in close geographic proximity, either sourced from different portions of the same magma system at depth or from discrete, uncommunicating bodies; (5) ambiguity with respect to whether or not CVF magmatism is time-predictable, as previously suggested, or erupted as a series of punctuated episodes; (6) no rhyolite volcanism in the past ~78 kyr.
Dating lacustrine episodes in the eastern Sahara by the epimerization of isoleucine in ostrich eggshells
The eggshell of the African ostrich, Struthio camelus , closely approximates a closed system for the retention of indigenous proteinaceous residues. Epimerization of the protein amino acid isoleucine follows linear first-order kinetics in laboratory simulations nearly to racemic equilibrium, and the variation in D/L ratio within a single fragment, or between fragments of the same age, is significantly less than in other carbonate systems. These observations suggest that the extent of isoleucine epimerization (aIle/Ile ratio) in ostrich eggshell offers the potential for high-resolution geochronology of Quaternary deposits. From the simulation experiments, and dated early Holocene samples for which we have in situ mean annual sediment temperature measurements, Arrhenius parameters have been calculated; the activation energy is 30.33 kcal mol −1 , similar to that of other carbonate systems. We have measured the aIle/Ile ratio in ostrich eggshell associated with lacustrine episodes at Bir Tarfawi and Bir Sahara East, two depressions in what is currently the hyperarid eastern Sahara. The ratios can be used directly to indicate qualitatively the time represented by each series of lake sediment, and to correlate disjunct lacustrine deposits within and between the basins. Uranium-series disequilibrium dating of algal mats contained within some of the lake beds indicate that a major wet interval occurred about 130 ka ago. Using the U-series date for calibration, the amino acid ratios are used to date the most recent lacustrine interval to about 100 ka B.P., and two older intervals, one about 200 ± 25 ka B.P., and an older interval that occurred prior to 250 ka ago.
Stable C, O and clumped isotope systematics and 14C geochronology of carbonates from the Quaternary Chewaucan closed-basin lake system, Great Basin, USA: Implications for paleoenvironmental reconstructions using carbonates
Isotopic compositions of lacustrine carbonates are commonly used for dating and paleoenvironmental reconstructions. Here we use carbonate δ13C and δ18O, clumped (Δ47), and 14C compositions to better understand the carbonate isotope system in closed-basin lakes and trace the paleohydrologic and temperature evolution in the Chewaucan closed-basin lake system, northern Great Basin, USA, over the Last Glacial/Holocene transition. We focus on shorezone tufas to establish that they form in isotopic equilibrium with lake water and DIC, they can be dated reliably using 14C, and their clumped isotope composition can be used to reconstruct past lake temperature. Calculations of the DIC budget and reservoir age for the lake indicate residence time is short, and dominated by exchange with atmospheric CO2 at all past lake levels. Modern lake DIC and shorezone tufas yield δ13C and 14C values consistent with isotopic equilibrium with recent fossil fuel and bomb-influenced atmospheric CO2, supporting these calculations. δ13C values of fossil tufas are also consistent with isotopic equilibrium with pre-industrial atmospheric CO2 at all shoreline elevations. This indicates that the 14C reservoir effect for this material is negligible. Clumped isotope (Δ47) results indicate shorezone tufas record mean annual lake temperature. Modern (average 13 ± 2 °C) and 18 ka BP-age tufas (average 6 ± 2 °C) have significantly different temperatures consistent with mean annual temperature lowering of 7 ± 3 °C (1 SE) under full glacial conditions. For shorezone tufas and other lake carbonates, including spring mounds, mollusk shells, and ostracod tests, overall δ13C and δ18O values co-vary according to the relative contribution of spring and lacustrine end member DIC and water compositions in the drainage system, but specific isotope values depend strongly upon sample context and are not well correlated with past lake depth. This contrasts with the interpretation that carbonate isotopes in closed-basin lake systems reflect changes in DIC and water budgets connected to higher or lower lake volumes. Instead, a small overlapping range of isotope compositions characterize multiple lake levels, so that none can be identified uniquely by isotope composition alone. Relative to other lake carbonates, δ13C and δ18O values for ostracods in Ana River Canyon deposits are very strongly influenced by Ana River water, suggesting low lake level and volume characterized Summer Lake for most of the past 100,000 years. Coupled with sedimentologic observations, the Ana River deposits thus suggest dry conditions like today are close to the mean climate state in the northern Great Basin. By contrast, basin-integrating highstands such as that dating to ∼14 ka BP, during the last glacial termination, are hydrologically unique and short-lived. Overall, our results indicate carbonate isotope records must account for the specific geochemical and hydrologic characteristics of lake system in order to provide robust paleoenvironmental reconstructions.
An optical age chronology of late Quaternary extreme fluvial events recorded in Ugandan dambo soils
There is little geochonological data on sedimentation in dambos (seasonally saturated, channel-less valley floors) found throughout Central and Southern Africa. Radiocarbon dating is problematic for dambos due to (i) oxidation of organic materials during dry seasons; and (ii) the potential for contemporary biological contamination of near-surface sediments. However, for luminescence dating the equatorial site and semi-arid climate facilitate grain bleaching, while the gentle terrain ensures shallow water columns, low turbidity, and relatively long surface exposures for transported grains prior to deposition and burial. For this study, we focused on dating sandy strata (indicative of high-energy fluvial events) at various positions and depths within a second-order dambo in central Uganda. Blue-light quartz optically stimulated luminescences (OSL) ages were compared with infrared stimulated luminescence (IRSL) and thermoluminescence (TL) ages from finer grains in the same sample. A total of 8 samples were dated, with 6 intervals obtained at ???35, 33, 16, 10.4, 8.4, and 5.9 ka. In general, luminescence ages were stratigraphically, geomorphically and ordinally consistent and most blue-light OSL ages could be correlated with well-dated climatic events registered either in Greenland ice cores or Lake Victoria sediments. Based upon OSL age correlations, we theorize that extreme fluvial dambo events occur primarily during relatively wet periods, often preceding humid-to-arid transitions. The optical ages reported in this study provide the first detailed chronology of dambo sedimentation, and we anticipate that further dambo work could provide a wealth of information on the paleohydrology of Central and Southern Africa. ?? 2006 Elsevier Ltd. All rights reserved.
Modeled tephra ages from lake sediments, base of Redoubt Volcano, Alaska
A 5.6-m-long lake sediment core from Bear Lake, Alaska, located 22 km southeast of Redoubt Volcano, contains 67 tephra layers deposited over the last 8750 cal yr, comprising 15% of the total thickness of recovered sediment. Using 12 AMS 14C ages, along with the 137Cs and 210Pb activities of recent sediment, we evaluated different models to determine the age-depth relation of the core, and to determine the age of each tephra deposit. The selected age model is based on a mixed-effect regression that was passed through the adjusted tephra-free depth of each dated layer. The estimated age uncertainty of the 67 tephras averages ??105 yr (95% confidence intervals). Tephra-fall frequency at Bear Lake was among the highest during the past 500 yr, with eight tephras deposited compared to an average of 3.7/500 yr over the last 8500 yr. Other periods of increased tephra fall occurred 2500-3500, 4500-5000, and 7000-7500 cal yr. Our record suggests that Bear Lake experienced extended periods (1000-2000 yr) of increased tephra fall separated by shorter periods (500-1000 yr) of apparent quiescence. The Bear Lake sediment core affords the most comprehensive tephrochronology from the base of the Redoubt Volcano to date, with an average tephra-fall frequency of one every 130 yr. ?? 2007 Elsevier Ltd. All rights reserved.
A revised burial dose estimation procedure for optical dating of youngand modern-age sediments
The presence of genuinely zero-age or near-zero-age grains in modern-age and very young samples poses a problem for many existing burial dose estimation procedures used in optical (optically stimulated luminescence, OSL) dating. This difficulty currently necessitates consideration of relatively simplistic and statistically inferior age models. In this study, we investigate the potential for using modified versions of the statistical age models of Galbraith et??al. [Galbraith, R.F., Roberts, R.G., Laslett, G.M., Yoshida, H., Olley, J.M., 1999. Optical dating of single and multiple grains of quartz from Jinmium rock shelter, northern Australia: Part I, experimental design and statistical models. Archaeometry 41, 339-364.] to provide reliable equivalent dose (D e ) estimates for young and modern-age samples that display negative, zero or near-zero D e estimates. For this purpose, we have revised the original versions of the central and minimum age models, which are based on log-transformed D e values, so that they can be applied to un-logged D e estimates and their associated absolute standard errors. The suitability of these 'un-logged' age models is tested using a series of known-age fluvial samples deposited within two arroyo systems from the American Southwest. The un-logged age models provide accurate burial doses and final OSL ages for roughly three-quarters of the total number of samples considered in this study. Sensitivity tests reveal that the un-logged versions of the central and minimum age models are capable of producing accurate burial dose estimates for modern-age and very young (<350??yr) fluvial samples that contain (i) more than 20% of well-bleached grains in their D e distributions, or (ii) smaller sub-populations of well-bleached grains for which the D e values are known with high precision. Our results indicate that the original (log-transformed) versions of the central and minimum age models are still preferable for most routine dating applications, since these age models are better suited to the statistical properties of typical single-grain and multi-grain single-aliquot D e datasets. However, the unique error properties of modern-age samples, combined with the problems of calculating natural logarithms of negative or zero-Gy D e values, mean that the un-logged versions of the central and minimum age models currently offer the most suitable means of deriving accurate burial dose estimates for very young and modern-age samples. ?? 2009 Elsevier Ltd. All rights reserved.
Radiocarbon dating of small terrestrial gastropod shells in North America
Fossil shells of small terrestrial gastropods are commonly preserved in wetland, alluvial, loess, and glacial deposits, as well as in sediments at many archeological sites. These shells are composed largely of aragonite (CaCO3) and potentially could be used for radiocarbon dating, but they must meet two criteria before their 14C ages can be considered to be reliable: (1) when gastropods are alive, the 14C activity of their shells must be in equilibrium with the 14C activity of the atmosphere, and (2) after burial, their shells must behave as closed systems with respect to carbon. To evaluate the first criterion, we conducted a comprehensive examination of the 14C content of the most common small terrestrial gastropods in North America, including 247 AMS measurements of modern shell material (3749 individual shells) from 46 different species. The modern gastropods that we analyzed were all collected from habitats on carbonate terrain and, therefore, the data presented here represent worst-case scenarios. In sum, ~78% of the shell aliquots that we analyzed did not contain dead carbon from limestone or other carbonate rocks even though it was readily available at all sites, 12% of the aliquots contained between 5 and 10% dead carbon, and a few (3% of the total) contained more than 10%. These results are significantly lower than the 20-30% dead carbon that has been reported previously for larger taxa living in carbonate terrain. For the second criterion, we report a case study from the American Midwest in which we analyzed fossil shells of small terrestrial gastropods (7 taxa; 18 AMS measurements; 173 individual shells) recovered from late-Pleistocene sediments. The fossil shells yielded 14C ages that were statistically indistinguishable from 14C ages of well-preserved plant macrofossils from the same stratum. Although just one site, these results suggest that small terrestrial gastropod shells may behave as closed systems with respect to carbon over geologic timescales. More work on this subject is needed, but if our case study site is representative of other sites, then fossil shells of some small terrestrial gastropods, including at least five common genera, Catinella, Columella, Discus, Gastrocopta, and Succinea, should yield reliable 14C ages, regardless of the local geologic substrate. ?? 2010.
Assessing the potential for luminescence dating of basalts
The possibility of dating basalt using luminescence was tested on four samples with independent age control from Cima volcanic field, California, with the ultimate aim of assessing whether the technique could be used to date sediments on the surface of Mars. Previous analysis of these samples had demonstrated that the infrared stimulated luminescence (IRSL) signal is most suitable for dating as it showed the lowest fading rate among various luminescence signals. In this study, changes in equivalent dose as a function of preheat are described. The ages for the two youngest Cima samples agree with the independent ages based on cosmogenic nuclide measurements (12.0 ± 0.8 ka). In the two older samples (dated to 320 and 580 ka by K–Ar), the luminescence behaviour is more complex and the form of the IRSL decay curve is seen to vary with dose. Mathematical fitting is used to isolate two components and their intensities are used to produce dose response curves. The slower component yields a larger equivalent dose. However, even using this component and after correction for fading, the ages obtained for the older samples are younger than the K–Ar ages.
Building on previous OSL dating techniques for gypsum: a case study from Salt Basin playa, New Mexico and Texas
The long term stability and reliability of the luminescence signal for gypsum has not been well documented or systematically measured until just recently. A review of the current literature for luminescence dating of gypsum is compiled here along with original efforts at dating an intact and in-situ bed of selenite gypsum at Salt Basin Playa, New Mexico and Texas. This effort differs from other documented luminescence dating efforts because the gypsum is not powdery or redistributed from its original growth patterns within the playa basin but is instead of a crystalline form. Sixteen ages from eight cores were ultimately produced with seven of the ages coming from rare detrital quartz encased in or with the gypsum crystals while the remaining ages are from the crystalline gypsum. As far as can be ascertained, the quartz was measured separately from the gypsum and no contaminants were noted in any of the aliquots. Some basic and preliminary tests of signal stability were measured and found to be mitigated by lessening of pre-heat protocols. Ages ranged from 8 ka to 10 ka in the shallow cores and 16 ka to 22 ka in the deeper cores. These ages will be useful in determining rates of gypsum growth within a sequence of evaporates which, in turn, will help to better document historic rates of evaporation and thus estimate, with more precision, the corresponding annual evaporation rates.