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USGS2025

USGS addresses needs for lithium calibration and quality control materials for pLIBS analysis

Lithium (Li) is a globally important commodity used for energy storage, national defense, human health, and advanced technologies. Lithium resource development requires identifying deposits with elevated concentrations and optimal mineralogy, typically associated with select clays and pegmatites. Lithium is a light, highly reactive alkali metal with low atomic mass that is difficult to detect and quantify using conventional portable geochemical techniques such as X-ray fluorescence (XRF). However, portable laser-induced breakdown spectroscopy (pLIBS) is a powerful analytical technique for lithium exploration due to its ability to analyze solids quickly with minimal preparation. The expanded utility of pLIBS is hampered by the lack of matrix-matched calibration and quality control (QC) materials. The United States Geological Survey (USGS) has developed in-house lithium calibration and QC materials for lithium in clay and pegmatite matrices to address this limitation. We present the workflow and implementation of a custom-built matrix specific calibration on a SciAps Z-300 pLIBS, using proprietary Profile Builder software. The implementation of the custom calibration and quality control standards enables us to collect semiquantitative results directly from the pLIBS while in the field. Ultimately, this calibration has improved confidence in sample selection and collection in the field, providing more efficient site characterization.

Conference Paper↗
USGS2025

Megafaunal community structure on ferromanganese and phosphorite hardgrounds in the Southern California Borderland

The Southern California Borderland (SCB) is a topographically complex region on the active continental margin that hosts varied hardground habitats, including ferromanganese (FeMn) crusts and phosphorites, marine minerals being considered for resource extraction. The SCB is influenced by seasonal upwelling and terrestrial inputs, and has a well-defined oxygen-minimum zone (OMZ). We analyzed megafaunal community composition, density, and diversity across 41 ROV video transects at 10 SCB hard substrate sites spanning depth (378–2765 m), temperature (1.79–7.96 °C), and oxygen (3.91–105.67 μM) gradients, with varying rock types (FeMn crusts, phosphorites, other rocks). We counted 32,426 individuals representing 146 unique taxa over a total area of 21,935 m 2 . Echinodermata contributed 48 % of the total abundance; Cnidaria 24 %; Porifera 13 %; Annelida 6 %; Arthropoda 6 %; Chordata 2 %; Mollusca, Foraminifera, and Hemichordata <1 %. Megafauna communities showed clear heterogeneity, with density, diversity, and community composition varying among transects within sites and across sites. Rock type recorded no influence on megafaunal density, but habitats that included FeMn crusts had higher diversity and distinct taxonomic composition. Location, depth, and oxygen were the most important variables explaining variance among megafaunal communities, with distinct communities formed at deeper depths and within the OMZ. This study provides baseline information about the megafauna inhabiting SCB hardgrounds, particularly those associated with minerals considered for their resource potential. It extends existing documentation of such communities to greater depths, reveals increased representation of sponges and corals below 1000 m, and highlights the variability within and among deep-sea megafaunal communities, offering context for informed policy decisions.

Southern California borderland↗
USGS2026

A novel drive-point multilevel system to investigate PFAS and other contaminants of global concern in the hyporheic zone of a wastewater effluent dominated stream

Contaminants found in treated wastewater discharged to streams, including pharmaceuticals and per- and polyfluoroalkyl substances (PFAS), are of global concern due to their deleterious effects on aquatic ecosystems and potential impacts to human health. Hyporheic zones have strong potential for contaminant attenuation. Assessing this potential requires collection of physical and biogeochemical data within the hyporheic zone. This study tested the applicability of a novel drive-point multilevel system (DP-MLS) for quantifying head profiles and characterizing contaminant concentrations in the hyporheic zone of a temperate region effluent dominated stream (EDS). DP-MLS, each with 4 ports, were installed in the stream bed at two sites, DS-1 and DS-2, 0.2 and 4.7 km downstream of the effluent outfall, respectively. Head profiles were measured and groundwater collected for analysis of pharmaceuticals and PFAS temporally over two years. The DP-MLS withstood rapid changes in stage, ice formation, and floating debris. Vertical hydraulic gradients (VHG) were generally upward but varied in magnitude indicating heterogeneity in hydraulic conductivity and variability in flow conditions. Upward VHG were also about 2X larger at DS-1 than at DS-2. Contaminant concentration profiles consistently showed penetration of pharmaceuticals and PFAS to 1 m below the bed at DS-2 while there was less penetration, lower groundwater concentrations, and more temporal variability in concentrations at DS-1. Integration of the physical and chemical data suggests weaker upwelling conditions at DS-2 are more easily reversed during periods of high stream stage, which could facilitate migration of wastewater contaminants into the bed. However, further studies incorporating other transport processes and reach scale dynamics are required to fully characterize these exchanges. Overall, this study demonstrates the efficacy of these novel DP-MLSs for characterization of the hyporheic zone and provides new insights into the occurrence, composition, and persistence of wastewater derived contaminants in the hyporheic zone of a well-studied EDS.

Iowa↗
USGS2025

Timing of hydrothermal alteration and Au-Sb-W mineralization, Stibnite-Yellow Pine district, Idaho

The Stibnite-Yellow Pine district of central Idaho was mined from the early 1900s until the 1990s, extracting gold, antimony, tungsten, and mercury from veins and disseminated and replacement ores in mountainous terrain along the headwaters of the Salmon River. Mining during the two World Wars supplied critical antimony and tungsten to the war efforts. Recent exploration has delineated mineral resources of over 187 metric tons Au, 274 metric tons Ag, and 93,000 metric tons Sb. Mineralization is hosted in Cretaceous Idaho batholith granitic rocks and a sequence of Neoproterozoic to Paleozoic metasedimentary strata of carbonate and siliciclastic compositions. Historical studies outlined some of the complex paragenesis but debated the absolute age of mineralization. New petrographic and geochronologic work documents a sequence of five hydrothermal events in the Stibnite-Yellow Pine district. Event 1 is related to Cretaceous magmatic and hydrothermal activity and includes events ranging in age from 86 to 75 Ma, including sparse quartz-molybdenite veins dated at 86 Ma. Disseminated gold mineralization of event 2 is associated with sericitic alteration and sulfidation of igneous biotite and replacement of plagioclase by potassium feldspar, largely in granodiorite. Gold is present in zoned arsenian pyrite in both disseminated ores and in crosscutting carbonate-quartz veins containing pyrite and arsenopyrite. The large Yellow Pine deposit, localized at a dilatant bend in the Meadow Creek fault, hosts such disseminated and vein gold. Event 2 is interpreted as the major gold-forming event; 40 Ar/ 39 Ar ages of sericite and potassium feldspar alteration range, respectively, from 70 to 59 and 66 to 56 Ma. The long span is interpreted to reflect the age of gold mineralization and local overprinting by event 3. A narrower range from 66 to 61 Ma is interpreted to date the peak of gold mineralization and alteration. Event 3, tungsten mineralization with scheelite, is texturally later than event 2 gold and localized along the Meadow Creek structure. Event 3 scheelite has been dated by isotope dilution-thermal ionization mass spectrometry (ID-TIMS) and laser ablation-inductively coupled plasma-mass spectrometry (LA-ICP-MS) U-Pb methods at 57 Ma. Event 4, best developed in the West End area, includes gold-silver–bearing quartz-carbonate-pyrite veins and breccias with epithermal textures and potassium feldspar alteration envelopes. Adularia from event 4 yields 40 Ar/ 39 Ar plateau ages of 52 to 51 Ma. Event 5 antimony and mercury mineralization consists of stibnite veins and breccia cements at the Yellow Pine and Hangar Flat deposits as well as cinnabar veins and replacements at the peripheral Fern and Hermes deposits; it is constrained by an LA-ICP-MS U-Pb date on scheelite (ca. 47 Ma) intergrown with stibnite. Minor propylitic and argillic alteration is evident in 47 Ma igneous dikes, which do not contain economic mineralization. The Au-Sb-W ores in the Stibnite-Yellow Pine mining district formed over an extended time period from about 70 to 45 Ma in multiple pulses that were localized along the Meadow Creek fault zone. Each event corresponds to episodes of magmatism and/or hydrothermal activity in the region. Insignificant event 1 skarn and molybdenum mineralization is similar in age to the Thompson Creek porphyry molybdenum deposit in central Idaho. Event 2 gold mineralization occurred during a magmatic gap in central Idaho but was synchronous with magmatism in the Bitterroot lobe further north; event 2 is similar in age to orogenic gold-arsenic mineralization at the Beartrack mine in eastern Idaho. Event 3 scheelite mineralization coincides with tungsten mineralization at the Quartz Creek deposit, late magmatism in the Bitterroot lobe, and rapid exhumation of the Atlanta lobe of the Idaho batholith. Event 4 gold mineralization is coincident with the onset of regional Challis magmatism and extension. Event 5 antimony and mercury mineralization is time-equivalent to epithermal gold mineralization in the nearby Thunder Mountain volcanic field and the peak of Challis magmatism.

Idaho↗
USGS1976

Geology and mineral deposits of the Needle Mountains District, Southwestern Colorado

The Needle Mountains district is set in highly fractured Precambrian granitic rocks that have intruded and metamorphosed older Precambrian metasedimentary rocks. The Precambrian rocks are overlain by outliers of Paleozoic strata and intruded by a late Tertiary stock. Past mineral production reportedly was limited to silver and gold ores presumably taken from small fissure veins. Although the economic potential of the district has not been adequately explored, some evidence indicates potential for base metal deposits.

Colorado↗
USGS2025

Three-dimensional seismic velocity models for the San Francisco Bay region, California from joint body-wave and surface-wave tomography validated by waveform simulation

A high-resolution seismic velocity model for both P and S waves is essential for the San Francisco Bay (SFB) region to accurately simulate earthquake ground motions and assess seismic hazards in this high-risk region. We present new three-dimensional P-wave and S-wave velocity (Vp and Vs) models of the SFB region developed using joint tomographic inversion with a rich set of earthquake and active-source body-wave data and ambient-noise surface-wave data. We designed a dynamic balance strategy to effectively balance the contributions of body-wave and surface-wave data during each iteration of the inversion. Owing to the complementary resolution of body-wave and surface-wave data, our new models are significantly improved compared to previous tomographic models. Major geologic features in the SFB region, including low-velocity basins, high-velocity Franciscan Complex, granite, and gabbro rocks, and across-fault velocity contrasts, are imaged in our Vp and Vs models. Compared to the geology-based U.S. Geological Survey velocity model, our new model has better defined structures for some important areas that are of great concern for seismic hazard assessment, such as the Sacramento-San Joaquin Delta, and the 2014 magnitude 6.0 South Napa earthquake area. We validated our model by simulating waveforms for a set of moderate-magnitude earthquakes. The good performance of our model in waveform simulation indicates its potential for improving ground motion simulation and seismic hazard assessment in the SFB region.

California↗
USGS2026

Cajon Pass and the southern San Andreas Fault System: Earthquake cycle stress accumulation and present-day loading

With over a century since the last major rupture affecting the wider Los Angeles region, tectonic stress has steadily built along the southern San Andreas and San Jacinto fault systems, raising concerns of an imminent large earthquake. Cajon Pass, located at the junction of these faults, represents a critical site for potential through-going ruptures in Southern California. We constructed new 4D earthquake cycle simulations using a 1000-year paleoseismic rupture history of the San Andreas Fault System (SAFS) to assess spatial and temporal variations in stress. A semi-analytic Fourier transform model was used to compute stress from 3D dislocations in an elastic plate overlying a Maxwell viscoelastic half-space, assuming a complete coseismic reset of resolved shear stress on ruptured elements. Results show highest stress accumulation north of Cajon Pass (∼1.8 MPa/100 years) due to greater slip rates, and lower rates south of Cajon Pass (∼1.0–1.5 MPa/100 years). By 2025, Coulomb stress is estimated at 2.8 MPa on the Mojave South (MOS) segment, 1.8 MPa on the North San Bernardino (NSB1) segment and 3.6 MPa on the San Jacinto Bernardino (SJB) segment. Segments accumulate stresses with characteristic ranges of pre-event stress interpreted as failure thresholds: 1.2–2.7 MPa for MOS, 0.4–1.6 MPa for NSB1, and 1.2–2.9 MPa for SJB. When the stress disparity between segments SJB and MOS narrows, the faults appear to rupture jointly, suggesting that stress levels may control how Cajon Pass acts as an earthquake gate. These results may inform seismic hazard assessments by linking stress evolution to fault interactions.

California↗
USGS2024

Relatively stable pressure effects and time-increasing thermal contraction control Heber geothermal field deformation

Due to geological complexities and observational gaps, it is challenging to identify the governing physical processes of geothermal field deformation including ground subsidence and earthquakes. In the west and east regions of the Heber Geothermal Field (HGF), decade-long subsidence was occurring despite injection of heat-depleted brines, along with transient reversals between uplift and subsidence. These observed phenomena contradict current knowledge that injection leads to surface uplift. Here we show that high-yield production wells at the HGF center siphon fluid from surrounding regions, which can cause subsidence at low-rate injection locations. Moreover, the thermal contraction effect by cooling increases with time and eventually overwhelms the pressure effects of pressure fluctuation and poroelastic responses, which keep relatively stable during geothermal operations. The observed subsidence anomalies result from the siphoning effect and thermal contraction. We further demonstrate that thermal contraction dominates long-term trends of surface displacement and seismicity growth, while pressure effects drive near-instantaneous changes.

California↗
USGS2024

A history of cryohydrogeology modeling and recent advancements through the integration of solute transport

Groundwater flow systems and permafrost are interrelated because permafrost thaw enhances permeability, while groundwater flow can advect heat and accelerate permafrost thaw (McKenzie et al. 2021). Given amplified climate change in cold regions, there is renewed interest in ‘cryohydrogeology’, the study of groundwater in cold regions. Many data-driven studies have shown that permafrost thaw is leading to activated aquifers and increased baseflow across the pan-Arctic region (e.g. Walvoord and Striegl 2007, Evans et al. 2020). Empirical evidence of a subsurface ‘replumbing’ (Walvoord and Kurylyk 2016) in permafrost regions raises questions about the fate of sequestered contaminants in the North (Langer et al. 2023). We will discuss the history of and emerging opportunities in cryohydrogeological modeling, with a focus on recent contaminant transport modeling.

Conference Paper↗
USGS2026

Guidelines for producing integrated 210Pb and 14C age-models

Accurate reconstructions of past environmental changes are crucial in paleoecological research and require reliable chronologies of sedimentary archives. Establishing robust age-models and obtaining the most appropriate proxies for analysis is a complex scientific endeavor, requiring extensive resources and collaboration among specialists, including radiochronologists. Radiometric dating methods, such as 210 Pb and radiocarbon ( 14 C), are frequently employed to establish chronologies in aquatic sedimentary deposits and peat bogs. In this study, we review key aspects of sampling, analysis, and the principles underlying 210 Pb and 14 C age-models, focusing on methods for developing robust joint chronologies for paleoenvironmental research. Drawing largely from the authors' experiences and group discussions during and after a scientific workshop in 2022, we discuss important considerations for site selection, sampling strategies, and radiometric dating to construct integrated 210 Pb and 14 C age-models. Using expert consensus, this group – called Paleostats – aims to provide a set of best practices for other geochronologists with this methods paper. Among our conclusions, we emphasize the importance of accounting for site-specific factors such as prior information on sedimentation rates to establish appropriate sampling and analytical strategies. The use of appropriate coring devices can minimize disturbance to sediments and ensure the core surface remains intact and preserved until sectioning. Where excess 210 Pb is expected, sectioning at intervals of ≤1 cm provides an adequate sampling resolution for 210 Pb dating. Exceptions are possible, allowing for ~2–3 cm sections in areas with confirmed high sedimentation rates (e.g., > 1 cm yr −1 ). Recovering deeper core sections for 14 C dating with sufficient overlap allows for accounting errors in depth estimates made in the field. Special attention is advised during time intervals where validation proxies, such as the human-made radionuclides 137 Cs or post-bomb 14 C, are expected, and to determine the depth of secular equilibrium between 210 Pb and 226 Ra. Radiocarbon analyses are commonly performed by accelerator mass spectrometry, and age models are constructed mainly using Bayesian statistics with Markov Chain Monte Carlo techniques (e.g., Bacon ). A Bayesian approach ( Plum ) is now available for producing 210 Pb age-models, which infers the 210 Pb ex flux, eliminates the need for selecting an equilibrium depth, and allows dating cores with incomplete 210 Pb ex inventory. Plum offers improved chronologies by integrating raw 210 Pb and 14 C data, and these age-models can be enriched with other dating methodologies, such as identifying tephras and other well-recorded historical events. Harmonized reporting would contribute to making radiometric age-models reproducible, which would benefit from an international effort. Using 210 Pb and 14 C to produce integrated age-models may yield better insights into the interplay between natural and recent anthropogenic forcings on ecosystems. This can enhance our understanding of environmental processes and their impacts on climate change, ultimately supporting science-based assessments and decisions.

Earth-Science Reviews↗
USGS2024

Surficial geology and Quaternary fault map of the Las Vegas Valley, Clark County, Nevada

The Surficial Geology and Quaternary Fault Map of the Las Vegas Valley, Clark County, Nevada is a 1:50,000-scale compilation of published 1:24,000-scale geologic maps integrated with new field and desktop mapping. This geologic map compilation and GIS database are part of a broader study on the Quaternary faults in the Las Vegas Valley, the results of which are summarized in this report. The map compilation utilized a variety of digital base maps to evaluate the characteristics of surficial deposits and Quaternary fault scarps including lidar data in undeveloped parts of the valley and orthorectified historical aerial photos in the urbanized center of the valley. The map distinguishes twenty surficial map units including alluvial-fan and ephemeral-wash deposits, groundwater discharge deposits of the Las Vegas Formation, and alluvium deposits of Las Vegas Wash. Quaternary faults include the Quaternary Las Vegas Valley fault system in the center of the valley and the Frenchman Mountain fault system along the eastern margin. All Quaternary fault traces in the valley were evaluated, and the previously published fault mapping was modified as needed. The new mapping and uniform correlation of surficial deposits displaced by Quaternary faults yields a consistent valley-wide characterization of the recency of fault activity. The map and GIS database include a Quaternary geochronology compilation of 119 previously published surficial deposit ages of various types, 35 new luminescence ages, and 3 new radiocarbon ages. The new age data further bracket the ages of the Las Vegas basin Quaternary stratigraphy and provide new constraints on the timing of Quaternary fault activity.

Nevada↗
USGS2026

Creation of aerial camera system boresight installations in Bangor, Maine; Monroe, Louisiana; and Bassville Park, Florida

Aerial camera systems rely on boresights for defining internal and external metrics. The U.S. Fish and Wildlife Service’s Migratory Bird Surveys Branch required boresights to calibrate their camera systems for creating georeferenced imagery that can then be used in geographic information systems. The U.S. Geological Survey created high-accuracy boresight installations in Bangor, Maine, in July 2024; Monroe, Louisiana, in September 2024; and Bassville Park, Florida, in January 2025 to provide this metric-defining capacity to the U.S. Fish and Wildlife Service. This U.S. Geological Survey Data Report details the methods and results of the boresight installation process and provides camera operators with the data needed to use each of the installations.

Florida, Louisiana, Maine↗
USGS2025

High-pass corner frequency selection and review tool for use in ground-motion processing

Raw seismological waveform data contain noise from the instrument’s surroundings and the instrument itself that can dominate recordings at low and high frequencies. To use these data in ground‐motion modeling, the effects of noise on the signals must be reduced and the signals’ usable frequency range identified. We present automated procedures to efficiently reduce low‐frequency noise that are implemented in the software package gmprocess. These procedures check for, and as needed remove, low‐frequency artifacts in the displacement record using polynomial fits, which can be used in combination with existing signal‐to‐noise ratio (SNR)‐based corner‐frequency selection procedures. The automated selections are then efficiently verified and refined using a graphical user interface (GUI) that plots relevant ground‐motion time series and spectra and tracks modifications to signal processing parameters. We demonstrate these procedures using recordings from the 2020 M 5.1 Sparta, North Carolina, and the 2013 M 4.7 southern Ontario earthquakes. Data processed with the SNR‐only and polynomial criteria for these events contain displacement artifacts in 37% and 23% of processed traces, respectively. Records with remaining artifacts are corrected manually using the GUI. These processing steps illustrate the workflow for efficient data processing with quality control.

Seismological Research Letters↗
USGS2025

U.S. Geological Survey science strategy to address white-nose syndrome and bat health in 2025–2029

Since its discovery in 2006, the fungal disease known as white-nose syndrome (WNS) has killed millions of bats. Of the 47 bat species native to the conterminous United States, Alaska, Hawaii, and Canada, 12 have been affected by WNS, including 3 endangered species and 1 proposed endangered species. WNS has also been detected in 40 States and 9 Canadian Provinces. U.S. Geological Survey (USGS) scientists have been critical in identifying the causal fungus for WNS ( Pseudogymnoascus destructans [Pd]), characterizing the effects of WNS, and tracking the spread of Pd in many bat populations in North America. The mission of the USGS WNS and Bat Health Science Team is to deliver integrated science in order to build resiliency into free-ranging bat populations through more effective WNS management, build capacity for bat health science, and enhance bat health information sharing across USGS science centers and cooperative research units as well as with stakeholders. The USGS can play an important role in supporting regional and national capacity building by providing resources and guidance to local, State, and Tribal management entities and by providing tools to enhance disease management. The USGS Ecosystems Mission Area’s Biological Threats and Invasive Species Research Program is the lead Federal program for free-ranging wildlife disease research and surveillance. As of 2024, guided by the science priorities set by the WNS Steering Committee, USGS scientists are engaged in a nationwide response to WNS. This work is done in close coordination with our partners at the U.S. Fish and Wildlife Service, National Park Service, Bureau of Land Management, U.S. Forest Service of the U.S. Department of Agriculture, U.S. Department of Defense, as well as State and Tribal agencies. In addition to conducting WNS research, the USGS is mapping the spread of WNS and coordinating the North American Bat Monitoring Program (NABat) to understand how WNS and other stressors affect the status and trends of native bats across their range. The USGS is supporting the national WNS response through four science goals: (1) provide situational awareness on the health of bat populations; (2) conduct ecological studies of bats along the gradient of disease vulnerability; (3) contribute actionable science to enhance the resiliency of bat populations; and (4) implement an adaptive, holistic approach to bat health.

Circular↗
USGS2024

Subduction zone geometry modulates the megathrust earthquake cycle: Magnitude, recurrence, and variability

Megathrust geometric properties exhibit some of the strongest correlations with maximum earthquake magnitude in global surveys of large subduction zone earthquakes, but the mechanisms through which fault geometry influences subduction earthquake cycle dynamics remain unresolved. Here, we develop 39 models of sequences of earthquakes and aseismic slip (SEAS) on variably-dipping planar and variably-curved nonplanar megathrusts using the volumetric, high-order accurate code tandem to account for fault curvature. We vary the dip, downdip curvature and width of the seismogenic zone to examine how slab geometry mechanically influences megathrust seismic cycles, including the size, variability, and interevent timing of earthquakes. Dip and curvature control characteristic slip styles primarily through their influence on seismogenic zone width: wider seismogenic zones allow shallowly-dipping megathrusts to host larger earthquakes than steeply-dipping ones. Under elevated pore pressure and less strongly velocity-weakening friction, all modeled fault geometries host uniform periodic ruptures. In contrast, shallowly-dipping and sharply-curved megathrusts host multi-period supercycles of slow-to-fast, small-to-large slip events under higher effective stresses and more strongly velocity-weakening friction. We discuss how subduction zones' maximum earthquake magnitudes may be primarily controlled by the dip and dimensions of the seismogenic zone, while second-order effects from structurally-derived mechanical heterogeneity modulate the recurrence frequency and timing of these events. Our results suggest that enhanced co- and interseismic strength and stress variability along the megathrust, such as induced near areas of high or heterogeneous fault curvature, limits how frequently large ruptures occur and may explain curved faults' tendency to host more frequent, smaller earthquakes than flat faults.

Journal of Geophysical Research: Solid Earth↗
USGS2025

Measurement of in situ-produced cosmogenic nuclides in fine-grained quartz from shale

In situ -produced 10 Be in quartz is widely used to constrain exposure ages and denudation rates, traditionally measured in sand-sized grains. Here we report a new method for isolating fine-grained quartz from shale and demonstrate its reliability for grain sizes down to single microns. Sequential dissolution tests and analyses of grain size separates show that meteoric 10 Be is eliminated and that recoil losses during cosmogenic nuclide production are balanced by implantation from other mineral grains. High-temperature combustion leads to diffusion of meteoric 10 Be into fine-grained quartz and must be used with caution.

Nuclear Instruments and Methods in Physics Researc↗
USGS2024

Geophysical characterization of an alkaline‑carbonatite complex using gravity and magnetic methods at Magnet Cove, Arkansas, USA

The Magnet Cove alkaline‑carbonatite complex (MCC), located in the Ouachita Mountains of south-central Arkansas in the United States, hosts an extensive variety of rare rock types and critical mineral resources with physical properties (density and magnetization) that contrast significantly with the sedimentary rocks into which they have intruded. Newly acquired ground-based gravity and magnetic data were used to develop two-dimensional and three-dimensional geophysical models of the Cretaceous-aged Magnet Cove intrusive complex. The models reveal that the MCC: (1) widens out at middle crustal depths to as much 22 km across, and may reach a depth of 20 km; (2) has a total volume (exposed and subsurface) that may be over 800 km 3 ; (3) is likely connected at depth to other intrusions in the Arkansas alkaline province; and (4) has a geometry that is aligned with pre-existing structures such as the Reelfoot rift and the Ouachita orogenic belt, some of which were likely structurally controlled by the Precambrian crystalline basement and the continent-ocean transition zone buried beneath the Ouachita orogen. For the first time, the magnetic models of the MCC account for the presence of strong remanent magnetization. This results in a geophysical workflow necessary to accurately interpret magnetic anomalies over the much larger Arkansas alkaline province, its geologic and structural framework, and critical mineral potential.

Arkansas↗
USGS2025

Using peak geometry and shifts in the x-ray spectrum of carbon from electron probe microanalysis to determine thermal maturity of organic matter

During the burial of mudstones, the associated organic matter undergoes gradual thermal maturation, a key process that can influence the reactivity of organic matter during catagenesis, the formation of hydrocarbon deposits and the chemical weathering of mudstones. Conventional methods for assessing the thermal maturity of organic matter often fail to reflect the geochemical heterogeneity between individual organic phases in mudstone samples. Here, we report an alternative, non-destructive, surficial and micro-scale (analytical spot size of ~ 300 nm with about 4 μm diffusion depth for micrometre-size organic grains) method to evaluate the thermal maturity of organic matter in mudstones using the carbon K α X-ray spectrum measured by field emission-electron probe microanalyser (FE-EPMA). Using this method, we observed correlations between parameter values derived from FE-EPMA spectra, including the peak position, the peak area and the intra-sample heterogeneity of these measurements, and independently measured vitrinite/solid bitumen reflectance for a suite of mudstones, representing different age, geological context and burial depth. With the increased values in peak area and position, we identified an increase in the carbon mass fraction of organic matter and the mean nominal oxidation state of carbon approaching zero. These trends, which are consistent with aromatisation and graphitisation, provide the rationale for using FE-EPMA to estimate the thermal maturity of organic matter. To explore some of these trends in more detail, we employed time-of-flight secondary ionisation mass spectrometry, X-ray photoelectron spectroscopy and optical reflectance measurements on a subset of samples.

Geostandards and Geoanalytical Research↗