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USGS1973

Inorganic chemical investigation by x-ray fluorescence analysis: The Viking Mars Lander

The inorganic chemical investigation added in August 1972 to the Viking Lander scientific package will utilize an energy-dispersive X-ray fluorescence spectrometer in which four sealed, gas-filled proportional counters will detect X-rays emitted from samples of the Martian surface materials irradiated by X-rays from radioisotope sources ( 55 Fe and 109 Cd). The output of the proportional counters will be subjected to pulse-height analysis by an on-board step-scanning single-channel analyzer with adjustable counting periods. The data will be returned to Earth, via the Viking Orbiter relay system, and the spectra constructed, calibrated, and interpreted here. The instrument is inside the Lander body, and samples are to be delivered to it by the Viking Lander Surface Sampler. Calibration standards are an integral part of the instrument. The results of the investigation will characterize the surface materials of Mars as to elemental composition with accuracies ranging from a few tens of parts per million (at the trace-element level) to a few percent (for major elements) depending on the element in question. Elements of atomic number 11 or less are determined only as a group, though useful estimates of their individual abundances maybe achieved by indirect means. The expected radiation environment will not seriously hamper the measurements. Based on the results, inferences can be drawn regarding (1) the surface mineralogy and lithology; (2) the nature of weathering processes, past and present, and the question of equilibrium between the atmosphere and the surface; and (3) the extent and type of differentiation that the planet has undergone. The Inorganic Chemical Investigation supports and is supported by most other Viking Science investigations.

Icarus↗

USGS1974

Naturally occurring vapor-liquid-solid (VLS) Whisker growth of germanium sulfide

The first naturally occurring terrestrial example of vapor-liquid-solid (VLS) growth has been observed in condensates from gases released by burning coal in culm banks. Scanning electron microscopy, X-ray diffraction, and energy dispersive analysis indicate that the crystals consist of elongated rods (≈ 100 μm) of germanium sulfide capped by bulbs depleted in germanium.

Journal of Crystal Growth↗

USGS1976

Holocene sedimentation history of the major fan valleys of Monterey fan

There are three major fan valleys on upper Monterey fan. Deep-tow geophysical profiles and 40 sediment cores provide the basis for evaluation of the sedimentation histories of these valleys. Monterey fan valley leads from Monterey canyon to a major suprafan and is bounded by levees that crest more than 400 m above the valley floor. The valley passes through a large z-bend or meander. Monterey East fan valley joins Monterey fan valley at the meander at about 150 m above the valley floor, and marks an earlier position of the lower Monterey fan valley. Ascension valley, a hanging contributary to the Monterey fan valley, appears to have once been the shoreward head of the lower part of the present Monterey fan valley. The relief of Monterey fan valley appears from deep-tow profiles to be erosional. The valley is floored with sand. Holocene turbidity currents do not overtop the levees 400 m above the valley floor, but do at times overflow and transport sand into Monterey East valley, producing a sandy floor. An 1100 m by 300 m dune field was observed on side scan sonar in Monterey East valley. Ascension fan valley was floored with sand during glacial intervals of lowered sea level, then was cut off from its sand source as sea level rose. A narrow (500 m), erosional, meandering channel was incised into the flat valley floor; the relief features otherwise appear depositional, with a hummocky topography perhaps produced in the manner of a braided riverbed. The sand is mantled by about 6 m of probable Holocene mud. Hummocky relief on the back side of the northwestern levees of both Ascension and Monterey valleys is characteristic of many turbidite valleys in the northeast Pacific. The hummocky topography is produced by dune-like features that migrate toward levee crests during growth.

California↗

USGS1980

Speculations on processes responsible for mesoscale current lineations on the continental shelf, southern California

A side-scan sonar survey of San Pedro shelf, California, reveals areas of mesoscale current lineations oriented approximately north-northeast in water depths of 20-25 m. Widths of sand ribbons range from 40 to 120 m and intervening erosional furrows, from 15 to 50 m. A conceptual model shows that the scale and orientation of current lineations agree with the dimensions and axial directions of Langmuir circulations theoretically generated by a combination either of southerly and southwesterly winds with regular trains of swell from the southern hemisphere or of two sets of wave trains crossing from the south and west. These longitudinal bedforms indicate shore-normal sediment transport at the times and on the areas of the shelf when and where they have been observed.

California↗

USGS1983

Geology of the head of Lydonia Canyon, U.S. Atlantic outer continental shelf

The geology of the part of Lydonia Canyon shoreward of the continental shelf edge on the southern side of Georges Bank was mapped using high-resolution seismic-reflection and side-scan sonar techniques and surface sediment grab samples. The head of the canyon incises Pleistocene deltaic deposits and Miocene shallow marine strata. Medium sand containing some coarse sand and gravel covers the shelf except for a belt of very fine sand containing no gravel on either side of the canyon in water depths of 125–140 m. Gravel and boulders, presumably ice-rafted debris, cover the rim of the canyon. The canyon floor and canyon wall gullies are covered by coarse silt of Holocene age which is as much as 25 m thick, and Miocene and Pleistocene strata are exposed on the spurs between gullies. The Holocene sediment is restricted to the canyon shoreward of the shelf edge and has been winnowed from the shelf. Furrows cut in the shelf sands and ripples on the shelf and in the canyon suggest that sediment continues to be moved in this area. Sediment distribution, however, is inconsistent with that expected from the inferred westward sediment transport on the shelf. Either the fine-grained deposits on the shelf to either side of the canyon head are relict or there is a significant component of offshore transport around the canyon head. In the head of Oceanographer Canyon, only 40 km west of Lydonia Canyon, present conditions are strikingly different. The floor of Oceanographer Canyon is covered by sand waves, and their presence indicates active reworking of the bottom sediments by strong currents. The close proximity of the two canyons suggests that the relative importance of processes acting in canyons can be variable over short distances.

Lydonia Canyon↗

USGS1987

Ice erosion of a sea-floor knickpoint at the inner edge of the stamukhi zone, Beaufort Sea, Alaska

In 1981 and 1982, detailed bathymetric and side-scan sonar surveys were made of an area of the sea floor north of Prudhoe Bay, Alaska, to study the changing characteristics of the seabed at the inner boundary of the stamukhi zone, the coast-parallel zone of grounded ice ridges that occurs in water depths between 15 and 50 m in the arctic. The fathograms and sonographs resolved 10-cm features and electronic navigation gave relocations accurate to about 10 m. Year after year an ice boundary develops at the inner edge of the stamukhi zone where major shear and pressure deformation occur in about the same location. Associated with this ice boundary, the bathymetry shows a pronounced break in slope — the knickpoint — on the shelf profile at about 20 m depth. The 2–3 m-high knickpoint is cut in a consolidated gravelly mud of pre-Holocene age. A well-defined gravel and cobble shoal a few meters high usually occurs at the inshore edge of the knickpoint. The sonograph mosaic shows that seaward of the knickpoint, ice gouges saturate the sea floor and are well defined; inshore the gouges are fewer in number and are poorly defined on the records. Few gouges can be traced from the seaward side of the knickpoint across the shoals to the inshore side of the knickpoint. Studies of ice gouging rates in two seabed corridors that cross the stamukhi zone reveal the highest rates of gouging seaward of the knickpoint. We believe that the knickpoint results from ice erosion at the inner boundary of the stamukhi zone. Intensified currents associated with this boundary winnow away fine sediments. Ice bulldozing and currents shape the shoals, which perch atop the knickpoint. The knickpoint helps to limit ice forces on the seabed inshore of the stamukhi zone.

Marine Geology↗

USGS1987

Seafloor gas seeps triggered by a northern California earthquake

A series of marine surveys using high-resolution seismic-reflection and side-scan sonar profiling was conducted on the Klamath River delta from 1977 to 1985. In November 1980, near the middle of this 8-year time period, a major earthquake (magnitude 7) occurred in the area. The earthquake caused liquefaction of shelf deposits off the Klamath River, and while mapping the sediment failures, we observed an inordinate number of gas vents and acoustic anomalies in the sediment (gas charging) and water column (gas clouds). Our analyses indicate that a change in gas seepage occurred after the earthquake. There was a marked increase in gas abundance immediately after the earthquake, a gradual decrease over the next year, and stabilization at pre-earthquake gas levels within five years or less. The acoustic anomalies were observed in pre-Quaternary rocks as well as in surficial Holocene deposits, and gas seeps overlay truncated anticlines, faults, and syncline exposures. Thus, the gas released may have been in part thermogenic in origin. A large area (20 km 2 ) on the delta failed during the earthquake, and the abundance of gas seeps and craters in the area suggests that sediment degassing may have been an important process contributing to failure.

Marine Geology↗

USGS1993

Neogene folding and faulting in southern Monterey Bay, Central California, USA

The goal of this study was to determine the Neogene structural history of southern Monterey Bay by mapping and correlating the shallow tectonic structures with previously identified deeper occurring structures. Side scan sonographs and Uniboom seismic reflection profiles collected in the region suggest that deformation associated with both compressional and transcurrent movement is occurring. Strike-slip movement between the North American and Pacific plates started as subduction ceased 21 Ma, creating the San Andreas fault system. Clockwise rotation of the Pacific plate occurred between 3.4 and 3.9 Ma causing orthogonal convergence between the two plates. This plate rotation is responsible for compressional Neogene structures along the central California coast. Structures exhibit transpressional tectonic characteristics such as thrust faulting, reverse faulting and asymmetrical folding. Folding and faulting are confined to middle Miocene and younger strata. Shallow Mesozoic granitic basement rocks either crop out or lie near the surface in most of the region and form a possible décollement along which the Miocene Monterey Formation has decoupled and been folded. Over 50% of the shallow faults strike normal (NE-SW) to the previously identified faults. Wrench fault tectonics complicated by compression, gradual uplift of the basement rocks, and a change in plate convergence direction are responsible for the observed structures in southern Monterey Bay.

Marine Geology↗

USGS1988

Fossil diatoms and neogene paleolimnology

Diatoms have played an important role in the development of Neogene continental biostratigraphy and paleolimnology since the mid-19th Century. The history of progress in Quaternary diatom biostratigraphy has developed as a result of improved coring techniques that enable sampling sediments beneath existing lakes coupled with improved chronological control (including radiometric dating and varve enumeration), improved statistical treatment of fossil diatom assemblages (from qualitative description to influx calculations of diatom numbers or volumes), and improved ecological information about analogous living diatom associations. The last factor, diatom ecology, is the most critical in many ways, but progresses slowly. Fortunately, statistical comparison of modern diatom assemblages and insightful studies of the nutrient requirements of some common freshwater species are enabling diatom paleolimnologists to make more detailed interpretations of the Quaternary record than had been possible earlier, and progress in the field of diatom biology and ecology will continue to refine paleolimnological studies. The greater age and geologic setting of Tertiary diatomaceous deposits has prompted their study in the contexts of geologic history, biochronology and evolution. The distribution of diatoms of marine affinities in continental deposits has given geologists insights about tectonism and sea-level change, and the distribution of distinctive (extinct?) diatoms has found utilization both in making stratigraphic correlations between outcrops of diatomaceous deposits and in various types of biochronological studies that involve dating deposits in different areas. A continental diatom biochronologic scheme will rely upon evolution, such as the appearance of new genera within a family, in combination with regional environmental changes that are responsible for the wide distribution of distinctive diatom species. The increased use of the scanning electron microscope for the detailed descriptions of fossil diatoms will provide the basis for making more accurate correlations and identifications, and the micromorphological detail for speculations about evolutionary relationships.

Palaeogeography, Palaeoclimatology, Palaeoecology↗

USGS1985

Digital image transformation and rectification of spacecraft and radar images

Digital image transformation and rectification can be described in three categories: (1) digital rectification of spacecraft pictures on workable stereoplotters; (2) digital correction of radar image geometry; and (3) digital reconstruction of shaded relief maps and perspective views including stereograms. Digital rectification can make high-oblique pictures workable on stereoplotters that would otherwise not accommodate such extreme tilt angles. It also enables panoramic line-scan geometry to be used to compile contour maps with photogrammetric plotters. Rectifications were digitally processed on both Viking Orbiter and Lander pictures of Mars as well as radar images taken by various radar systems. By merging digital terrain data with image data, perspective and three-dimensional views of Olympus Mons and Tithonium Chasma, also of Mars, are reconstructed through digital image processing. ?? 1985.

Photogrammetria↗

USGS1979

A herringbone bedform pattern of possible Taylor-Görtler type flow origin seen in sonographs

Side-scan sonar records collected in a shallow arctic lagoon (2–2.5 m depth) reveal a herringbone pattern of current-aligned linear reflectors with branching diagonals. The major longitudinal reflectors have no detectable relief (<20 cm), are spaced 5–10 m apart, and may represent current-aligned helical cell boundaries preserved in the silty fine sand of the lagoon floor. The pattern suggests a three-dimensional flow regime of the Taylor-Görtler type.

Sedimentary Geology↗

USGS1980

Identification of bedforms in lower Cook Inlet, Alaska

The seafloor of the central part of lower Cook Inlet, Alaska, is characterized by the presence of different sizes and types of bedforms. The bedforms in the sandy sediments include straight-crested to sinuous to lunate ripples, small, medium, and large sand waves, sand ridges, sand ribbons, and sand patches. In addition, rocky and pebbly seafloor has been identified. The water depth ranges from 25 to 120 m, and surface currents average 3.8 kt (2 m/s). Bottom currents have been measured at as much as 42 cm/s at 1 m above bottom. Underwater television observations have shown that the rate of sand transport is lower than expected because small amounts of clay and organic matter appear to inhibit remobilization. Only during the last 1 to 2 h of ebb and flood stages of spring tides, and during storms, does significant transport occur. Comparison of data from high-resolution seismic profiling systems, side-scan sonar, bottom television and camera, and bottom sampling shows that bottom and bedform interpretations based solely on sonographs can be in error. Measuring the length of ‘acoustic shadows’ on sonographs to obtain bedform heights gives dimensions that are too large by factors of 3–7. Bottom television investigations revealed that the troughs between small sand waves are flat and carpeted by shell fragments. Such coarse material has a high acoustic reflectance that is not related to slope or height and can lead to false interpretations on bedform dimensions. Our observations have shown that small sand waves commonly superimposed on larger ones are slightly higher than those present on flat hard bottom but are still less than calculated from acoustic shadows. Where the bottom is rather smooth or contains elevations small enough to be masked by bathymetric ‘noise’ caused by the pitching of the vessel, sonographs typically show either small sand waves, sand ribbons, sand patches, rocks, or smooth bottom. The smooth-bottom category can vary widely from ripples to gravelly or shelly or to small rocks with biological overgrowth as verified by television observations. Our observations have clearly demonstrated the need for an integrated multi-scale observation and sampling program in order to classify the bottom characteristics and to provide quantitative data for transport calculations.

Alaska↗

USGS1996

Contemporary channel-levee systems in active borderland basin plains, California Continental Borderland

Long-range large-scale side-scan (GLORIA) information, other seismic reflection profiling studies, and data from cores in the California Continental Borderland, have defined active levee-channel systems extending basinward from the lower fan of Hueneme-Mugu Submarine Fan, Redondo Submarine Fan, and Santa Cruz Canyon Fan in Santa Monica, San Pedro and Santa Cruz Basins, respectively. The Holocene distributaries have been created by a series of turbidity current events. These distributaries range in length from 10–25 km, and are wide (2–5 km) and low-relief (1–10 m) in their distal parts. They are also active conduits for nepheloid flows. Distributions of sedimentological parameters typically mimic the pattern of levee-channel systems. Organic carbon and biogenic carbonate content roughly outline the systems. Channels are incised in the upper to middle fan areas, and become constructional leveed channels in the lower fan and basin plain as the channel gradient adjusts to maintain a graded profile. Thus sediment gravity flows are generally confined to channels in the upper fan zones, but deposit both channelized and over-bank deposits on the lower fan and basin floor. The deposits show that the canyon-fan activity has continued during a rising sea level phase. It is evident that canyon headward erosion rates have been equal to or greater than the transgression rate, and that the canyon-fan systems have remained linked with their sediment sources. Frequency of events was probably higher, and volumes of the events were often larger, during the glacially lowered sea level episodes. However, turbidity currents of sufficient volume to reach the basin floors continue to occur at century or multi-century intervals. As one progresses headward in each system, the number of flows per length of core increases. Small flows that do not pass beyond the distributaries are much more frequent, and may be decadal in frequency, or even more frequent in the Santa Monica Basin system. These California borderland basins are probably typical of narrow active margins where rate of lateral sea level transgression is less than or equal to the rate of canyon headward erosion. The canyons maintain connections with sediment sources during sea level rise, and the systems therefore are active during the entire sea level cycle. Thus sediment supply is not a simple function of eustacy. This contrasts with the simplified sequence model developed on passive margins where canyons turn off as sea level rises.

California↗

USGS1989

Heat capacities and entropies from 8 to 1000 K of langbeinite (K 2 Mg 2 (SO 4 ) 3 ), anhydrite (CaSO 4 ) and of gypsum (CaSO 4 ·2H 2 O)

Heat capacities of K 2 Mg 2 (SO 4 ) 3 (langbeinite) and CaSO 4 (anhydrite) were measured from approximately 8 to 1000 K by combined adiabatic shield calorimetry (8-365 K) and differential scanning calorimetry (350-1000 K). Heat capacities were also measured on natural crystals of gypsum (CaSO 4 · 2H 2 O) between 8.1 and 323.5 K. The molar entropies at 298.15 K, S m o (298.15 K), are 378.8 ± 0.6, 107.4 ± 0.2 and 193.8 ± 0.3 J K −1 mol −1 for langbeinite, anhydrite and gypsum, respectively. The heat capacity in J K −1 mol −1 of langbeinite can be represented by the equation C p,m o (K 2 Mg 2 (SO 4 ) 3 T ) = 535.9 + 0.11011 T -1.0200 × 10 6 / T 2 -4.909 × 10 −5 T 2 -4040.2/ T 0.5 between 300 and 1000 K with an average deviation of ± 0.4%. For anhydrite the heat capacity between 300 and 1000 K is given by C p,m o (CaSO 4 , T ) = 372.8 - 0.1574 T +1.695 × 10 6 / T 2 + 7.993 × 10 −5 T 2 - 4330.8/ T 0.5 with an average deviation of ±0.4%. Combining our heat-capacity and entropy data with the solution calorimetric results of Kelley et al. (U.S. Bur. Mines Tech. Paper, 625, 1941) yields an equilibrium temperature for the reaction gypsum → anhydrite + 2 water of 314.7 K (41.5 ° C). Our observations are in agreement with the conclusions of Speer and Salje (Phys. Chem. Miner., 13 (1986) 17); we see no evidence in our heat capacity measurements for the transformation of cubic langbeinite (P2 1 3) to a low temperature orthorhombic (P2 1 2 1 2 1 ) form as is seen in the isostructural Co, Zn, Ca, Mn and Cd langbeinites. Although Bond (Bell Sys. Tech. J., 22 (1943) 145) reported that langbeinite was piezoelectric at room temperature, we found no evidence in our C p o measurements for a Curie temperature above which langbeinite would no longer be piezoelectric.

Thermochimica Acta↗

USGS1993

Differentiation of volcanic ash-fall and water-borne detrital layers in the Eocene Senakin coal bed, Tanjung Formation, Indonesia

The Sangsang deposit of the Eocene Senakin coal bed, Tanjung Formation, southeastern Kalimantan, Indonesia, contains 11 layers, which are thin (<5 cm) and high in ash (> 70%). These layers are characterized by their pelitic macroscopic texture. Examination of eight of the layers by scanning-electron microscopy, energy-dispersive X-ray, and X-ray diffraction analyses show that they are composed primarily of fairly well-crystallized kaolinite, much of which is vermicular. Accessory minerals include abundant Ti oxide, rare-earth element-rich Ca and A1 phosphates, quartz that luminescences in the blue color range, and euhedral to subhedral pyroxene, hornblende, zircon, and sanidine. Although this mineral suite is suggestive of volcanic ash-fall material, only the four pelitic layers in the middle of the bed are thought to be solely derived from volcanic ash-falls on the basis of diagnostic minerals, replaced glass shards, and lithostratigraphic relationships observed in core and outcrop. The three uppermost pelitic layers contain octahedral chromites, some quartz grains that luminesce in teh orange color range, and some quartz grains that contain two-phase fluid inclusions. These layers are interpreted to be derived from a combination of volcanic ash-fall material and hydrologic transport of volcaniclastic sediment. In contrast, the lowermost pelitic layer, which contains large, rounded FeMg-rich chromites, is thought to have been dominantly deposited by water. The source of the volcanic ash-fall material may have been middle Tertiary volcanism related to plate tectonic activity between Kalimantan and Sulawesi. The volcanic ash was deposited in sufficient amounts to be preserved as layers within the coal only in the northern portions of the Senakin region: the southern coal beds in the region do not contain pelitic layers.

southeastern Kalimantan↗

USGS1993

SEM-EDX and isotope characterization of the organic sulfur in macerals and chars in Illinois Basin coals

Two samples of the Herrin (Illinois No. 6) Coal and one sample of the Colchester (Illinois No. 2) Coal from the Illinois Basin were studied to evaluate the spatial distribution of organic sulfur within macerals occurring next to pyrite grains, both in the raw coal and their chars. The chars were produced by pyrolysing the coal at 250–550°C in a nitrogen atmosphere. Representative splits of the coals and their chars were mounted in epoxy and polished for optical microscopy and scanning electron microscopy-energy dispersive x-ray spectroscopy (SEM-EDX). Determinations of organic sulfur concentrations were made at 996 locations within macerals, mostly vitrinite, around 115 grains of pyrite and at 50 locations around 5 pores in chars. The pyrite considered here is restricted to the disseminated type within macerals. On the average, the organic sulfur content increased near pyrite grains after the coals were charred at 550°C, indicating that some of the pyritic sulfur released during charring was retained within the organic matrix rather than being emitted to the atmosphere. One of the coal samples and its chars were isotopically characterized by chemically separating the pyritic and organic sulfur fractions, followed by analyzing the isotopes of the sulfur forms with a Nuclide 6–60 ratio mass spectrometer. The sulfur isotope (δ 34 S) data confirmed the movement of pyritic sulfur into the macerals after charring to 550°C. About 18% of the organic sulfur that remained in the 550°C char had originally been pyritic sulfur in the untreated coal.

Organic Geochemistry↗

USGS1993

Factors affecting the geochemistry of a thick, subbituminous coal bed in the Powder River Basin: Volcanic, detrital, and peat-forming processes

The inorganic geochemistry and mineralogy of three cores from the Anderson-Dietz 1 coal bed, a 15.2-m-thick subbituminous coal bed in the Tongue River Member (Paleocene) of the Fort Union Formation, were examined (1) to determine if the cores could be correlated by geochemical composition alone over a total distance of 2 km and (2) to identify the major factors that influenced the geochemistry of the coal bed. Chemical data (46 elements on a coal-ash basis) for 81 coal samples and 4 carbonaceous rock samples, with most samples representing a 0.6-m-thick (2-ft) interval of core, were grouped into compositional clusters by means of cluster analysis. Seven major clusters were produced; two of these clusters can be used to correlate the coal bed throughout the study area. Data from scanning electron and optical microscope analyses indicate that several factors influenced the geochemistry of the Anderson-Dietz 1 coal bed. The majority of mineral grains in the coal bed are interpreted to be detrital (water borne); evidence includes the presence of rounded to subrounded quartz grains having two-phase, aqueous fluid inclusions characteristic of hydrothermal or low-to-moderate grade metamorphic quartz. These quartz grains are found throughout the coal bed but are most abundant in samples from the midpart of the bed, which was influenced by detrital input associated with the deposition of the clastic rocks that form the split between the Anderson and Dietz 1 coal beds 900 m to the east of the study area. In addition to the detrital minerals mentioned above, volcanic ash that was fluvially transported to the sites of peat deposition or possibly deposited as air-fall volcanic ash also affected the geochemistry of the coal bed. For example, crandallite(?), a mineral reported to form as an alteration product of volcanic ash, is found in seven samples from the coal bed. The presence of quartz grains containing silicate-melt inclusions in eight samples from the coal bed.provides further support for a volcanic ash component. Other factors that probably affected the geochemistry of the coal bed include (1) detrital input associated with the deposition of the roof rocks of the coal bed, (2) peat-forming processes and plant material, and (3) epigenetic ground-water flow.

Montana, Wyoming↗

USGS1982

Recommended procedures and techniques for the petrographic description of bituminous coals

Modern coal petrology requires rapid and precise description of great numbers of coal core or bench samples in order to acquire the information required to understand and predict vertical and lateral variation of coal quality for correlation with coal-bed thickness, depositional environment, suitability for technological uses, etc. Procedures for coal description vary in accordance with the objectives of the description. To achieve our aim of acquiring the maximum amount of quantitative information within the shortest period of time, we have adopted a combined megascopic-microscopic procedure. Megascopic analysis is used to identify the distinctive lithologies present, and microscopic analysis is required only to describe representative examples of the mixed lithologies observed. This procedure greatly decreases the number of microscopic analyses needed for adequate description of a sample. For quantitative megascopic description of coal microlithotypes, microlithotype assemblages, and lithotypes, we use (V) for vitrite or vitrain, (E) for liptite, (I) for inertite or fusain, (M) for mineral layers or lenses other than iron sulfide, (S) for iron sulfide, and (X 1 ), (X 2 ), etc. for mixed lithologies. Microscopic description is expressed in terms of V representing the vitrinite maceral group, E the exinite group, I the inertinite group, and M mineral components. volume percentages are expressed as subscripts. Thus (V) 20 (V 80 E 10 I 5 M 5 ) 80 indicates a lithotype or assemblage of microlithotypes consisting of 20 vol. % vitrite and 80% of a mixed lithology having a modal maceral composition V 80 E 10 I 5 M 5 . This bulk composition can alternatively be recalculated and described as V 84 E 8 I 4 M 4 . To generate these quantitative data rapidly and accurately, we utilize an automated image analysis system (AIAS). Plots of VEIM data on easily constructed ternary diagrams provide readily comprehended illustrations of the range of modal composition of the lithologic units making up a given coal bed. The use of bulk-specific-gravity determinations is alo recommended for identification and characterization of the distinctive lithologic units. The availability of an AIAS also enhances the capability to acquire textural information. Ranges of size of maceral and mineral grains can be quickly and precisely determined by use of an AIAS. We assume that shape characteristics of coal particles can also be readily evaluated by automated image analysis, although this evaluation has not yet been attempted in our laboratory. Definitive data on the particulate mineral content of coal constitute another important segment of petrographic description. Characterization of mineral content may be accomplished by optical identification, electron microprobe analysis, X-ray diffraction, and scanning and transmission electron microscopy. Individual mineral grains in place in polished blocks or polished this sections, or separated from the coal matrix by sink-float methods are studied by analytical techniques appropriate to the conditions of sampling.

International Journal of Coal Geology↗