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Earth Mapping Resources Initiative protocols—Sampling hard-rock mine waste and perpetual mine water sources

Supporting the overarching goal to evaluate critical minerals nationwide, the mine waste characterization effort in the U.S. Geological Survey (USGS) Earth Mapping Resources Initiative has created a series of protocols to standardize sampling carried out under this effort by the participating State geological surveys and their cooperators. The protocols are based on published, reviewed methods that can be deployed in the field. The protocols include (1) collecting and processing composite samples of mine and mill waste, including tailings, waste rock, gangue, heap leach piles, ore stockpiles, slag, or other mineralized and processed materials and (2) collecting and preserving water samples from perpetual or long-term mine water sources. The protocols also specify information to document on field sheets and detail the collection of geospatial data. The analytical methods used by the USGS and USGS contract laboratories are described in this report, including the data delivery pathway for USGS-derived data.

Scientific Investigations Report

SUTRA— A code for simulation of saturated-unsaturated, variable-density groundwater flow with solute or energy transport—Documentation of the version 4.0 enhancements—Freeze-thaw capability, saturation and relative-permeability relations, spatially varying properties, and enhanced budget and velocity outputs

Version 4.0 of the Saturated-Unsaturated Transport (SUTRA) software code provides the capability to simulate the freezing and thawing of groundwater during energy transport simulations under saturated and unsaturated conditions. In addition to the types of hydrogeologic processes that SUTRA has been able to simulate in the past, this version can be used to study the effects of the freeze-thaw process on the flow and energy dynamics of hydrogeologic systems. The freeze-thaw simulation capability accounts for the latent heat of fusion and allows thermal property values to vary with changing total-water saturation, liquid-water saturation, and ice saturation. It allows the effective permeability of the porous medium to change as a result of freezing and thawing. This version also provides several user-selectable relations for the dependence of total-water saturation on fluid pressure, the dependence of liquid-water saturation on temperature during freezing and thawing, and the dependence of relative permeability on liquid saturation, as well as three user-selectable formulae for defining the bulk thermal conductivity of a mixture of solid grains, liquid water, ice, and air. For unsaturated simulations without freezing, the selectable total-water saturation relations eliminate the need for the user to program these and their associated relative-permeability functions, as had been required in previous SUTRA versions. Optional nonlinear dependence of fluid density on temperature, which covers the range from supercooled (about −50 degrees Celsius) to superheated (about 400 degrees Celsius), is also provided. Additionally, this version makes it possible to spatially vary parameters that, in previous versions of SUTRA, were required to be spatially uniform: solid-matrix properties, adsorption parameters, and parameters for production of solute mass or energy. Spatial variation is also allowed for the newly included freeze-thaw process parameters. Additional enhancements provide (1) output of water-mass and energy budgets that include values of all component terms in the governing balance equations, and (2) output of Darcy velocities (fluid fluxes), in addition to the velocity output provided by previous SUTRA versions. These enhanced outputs allow fuller interpretation of simulation results, especially for freeze-thaw phenomena. The set of processes simulated by this version of SUTRA are useful for studying a wide range of hydrogeologic system types, conditions, and questions. For cryohydrogeologic simulations, however, this version of the code is limited in that (1) it does not simulate thermomechanical effects of freeze-thaw, (2) pressure changes due to water density change during freezing are neglected, (3) ice saturation cannot exceed the initial porosity of the simulated medium, and (4) cryosuction, the migration of liquid water toward freezing fronts, is neglected. Furthermore, this version does not account for air flow or for water vaporization and sublimation under unsaturated conditions.

Techniques and Methods

Conceptual hydrogeologic framework and groundwater budget near the southeastern part of Puget Sound, Washington

More than 1 million people live within the active model area (AMA) in the southeastern part of the lowlands surrounding Puget Sound, or Puget Lowland, Washington, and groundwater is the source for approximately one-half of their public, domestic, and irrigation water demands. The 887-square-mile AMA, located in King and Pierce Counties, represents the area of analysis for the conceptual hydrogeologic framework and numerical groundwater-flow models within the study area and includes the Puyallup River and Chambers-Clover Creek watersheds. To assess the potential hydrologic and anthropogenic impacts to groundwater and the connected surface-water resources, conceptual and numerical groundwater-flow models of groundwater flow were developed by the U.S. Geological Survey Washington Water Science Center in close cooperation with 18 water-resource agencies and stakeholders. This report presents information used to characterize the groundwater-flow system and the development of a numerical model in the AMA. Included are descriptions of the geology and conceptual hydrogeologic framework, groundwater levels and flow directions, groundwater recharge and discharge, numerical groundwater-flow model construction and results, and model limitations. The study area encompasses the western part of Pierce County and the southwestern part of King County, Washington. The study area extends south to the Nisqually River, southwest to Tanwax Creek, northeast to the Green River, and north through the valley near Auburn and adjacent uplands. It is bounded on the east by foothills of the Cascade Range, and on the northwest by Puget Sound.

Washington

Standardized method for logging drill core at the Idaho National Laboratory, Idaho

The U.S. Geological Survey’s (USGS) Lithologic Core Storage Library (CSL) at the Idaho National Laboratory stores more than 120,000 feet of drill core that is accessible to the public for research and sampling. To effectively convey the physical and descriptive properties of the drill core, USGS staff at the Idaho National Laboratory Project Office log the drill core and publish the lithologic logs as data releases. The logs provide essential data on the lithology, texture, mineralogy, alteration, and other physical properties of the core, which serve as valuable information for researchers to guide their research and sampling efforts. To ensure consistent, quality, and dependable lithologic logs, this document outlines the procedures and expectations for logging drill core at the CSL. This document describes the processes for storing, photographing, and logging core, and includes a variety of resources, reference materials, and appendixes designed to standardize and aid the logging process. Following the procedures outlined in this document will produce consistent, detailed logs that facilitate dependable observations and serve as an easy reference for researchers and other interested parties.

Idaho

Avian navigation: Comparing the olfactory navigational “map” and the infrasound direction-finding hypotheses to aeronautics

Animal navigation has long been a fascinating but bewildering subject. Humans and animals might well share similar navigational strategies because they developed within the same physical environments. A “map-and-compass” model has been proposed to explain the two-step avian navigational process, but the “map” step has remained elusive. Although scalar values from bicoordinate geomagnetic or atmospheric olfactory gradients have been considered foundational to the avian map, neither has proved convincing engendering decades of controversy. The olfactory map, and an alternative infrasound direction-finding (IDF) hypothesis, are discussed in this review. The olfactory map hypothesis currently requires extensive stable gradients of trace-odor ratios, but such gradients are highly unlikely within a turbulent and rapidly mixed lower atmosphere. The IDF hypothesis, on the other hand, postulates a two-step navigational model analogous to the maritime and aeronautical radio direction-finding technique. This review was also written to encourage further investigation, and direct testing, of the acoustic navigational process. The IDF hypothesis, at present, appears the better explanation of observed avian navigational behavior and accuracy within the atmosphere’s physical environment.

Journal of Comparative Physiology A

Using the D-Claw software package to model lahars in the Middle Fork Nooksack River drainage and beyond, Mount Baker, Washington

Lahars, or volcanic mudflows, are the most hazardous eruption-related phenomena that will affect communities living along rivers that originate on Mount Baker. In the past 15,000 years, the largest lahars from Mount Baker have affected the Middle Fork Nooksack River drainage and beyond. Here we use the physics-based D-Claw software package to model nine lahar scenarios that are initiated as water-saturated landslides between Sherman Crater and the Roman Wall on the Mount Baker edifice and flow down the Middle Fork Nooksack River. The scenarios range in volume from 1 to 260 million cubic meters and have an initial hydraulic permeability from 10 −12 to 10 −10 meters squared. Model output includes data such as flow depth, velocity, runout distance, area inundated, arrival time, and sediment concentration as well as information that allows scientists to calculate other important hydrologic characteristics such as lahar discharge. These data are important to officials who have the responsibility to plan for, or take mitigation measures against, future Mount Baker lahars. To check the validity of the D-Claw results, we compare the scenarios to known geologic information. We also compare D-Claw results with empirical models that have been used in the past to determine potential inundation areas, runout distances, and arrival times. These comparisons highlight similarities and differences between empirical and physics-based models. We also present D-Claw scenario-based animations to help scientists, officials, and lay people alike to visualize how future lahars could affect communities.

Washington

Sedimentary exhalative (sedex) zinc-lead-silver deposit model

This report draws on previous syntheses and basic research studies of sedimentary exhalative (sedex) deposits to arrive at the defining criteria, both descriptive and genetic, for sedex-type deposits. Studies of the tectonic, sedimentary, and fluid evolution of modern and ancient sedimentary basins have also been used to select defining criteria. The focus here is on the geologic characteristics of sedex deposit-hosting basins that contain greater than 10 million metric tons of zinc and lead. The enormous size of sedex deposits strongly suggests that basin-scale geologic processes are involved in their formation. It follows that mass balance constraints of basinal processes can provide a conceptual underpinning for the evaluation of potential ore-forming mechanisms and the identification of geologic indicators for ore potential in specific sedimentary basins. Empirical data and a genetic understanding of the physicochemical, geologic, and mass balance conditions required for each of these elements are used to establish a hierarchy of quantifiable geologic criteria that can be used in U.S. Geological Survey national assessments. In addition, this report also provides a comprehensive evaluation of environmental considerations associated with the mining of sedex deposits.

Scientific Investigations Report

Measuring stress In high pressure deformation experiments with high speed fiber-optics

High‐pressure, high‐temperature rock deformation experiments are essential for understanding deep Earth processes, but accurately measuring stress is challenging due to the inaccuracy introduced by seal friction within the apparatus and large inertia, which affects earthquake process measurements made far from the experimental fault. To overcome these limitations, we developed and implemented a simple, compact fiber‐optic sensor based on an External Cavity Fabry–Perot Interferometer for in situ load measurement on a piston inside the pressure vessel of a Griggs‐type high‐pressure apparatus. The sensor can be used at sample temperatures up to 800°C for both slow creep and fast rupture testing with bandwidth capability from DC to 6 MHz. Two important experimental results are described: (1) the first direct measurements of seal friction in this apparatus type; these measurements record seal friction approximately one‐tenth of the confining pressure under both low (150 MPa) and high (1 GPa) pressure conditions; and (2) high‐temporal resolution capture of dynamic stress drops during stick‐slip faulting events at high‐confining pressure, revealing near‐fault wave propagation details, high‐frequency oscillations, and implying high‐transient slip rates (6–12 m/s) previously inaccessible with external sensors.

The Seismic Record

Public water-supply systems and water use in Tennessee, 1988

This report summarizes the results of a study conducted by the U.S. Geological Survey, in cooperation with the Tennessee Department of Environment and Conservation (TDEC), Division of Water Supply in 1988. Data gathered during an inventory by the TDEC were collated to determine water use, supply sources, population served, and design and storage capacities of the systems. The inventory was limited to systems that were active on June 30, 1988. Results of a survey of the systems conducted by the Tennessee Department of Health and Environment during 1988 were a primary source of data for this report. Data from computer and manual files maintained by the Tennessee Department of Health and Environment and the U.S. Geological Survey also were used. The Division of Water Supply, TDEC, surveyed 541 public water-supply systems. These systems served 81 percent of the population of the State, or 3.95 million people. The gross per capita use statewide for public-supplied water was 179 gallons per day. Total water withdrawals for public supply increased about 39 percent from 510 million gallons per day (Mgal/d) in 1980, to 708 Mgalld in 1988. During the same period, the population increased about 7 percent. Surface-water withdrawals accounted for 63 percent (446 Mgal/d) of the total water withdrawn in the State. All of these withdrawals occurred in the Tennessee (56 percent or 249 Mgal/d) and the Ohio (44 percent or 197 Mgalld) hydrologic regions. Ground water supplied 262 Mgal/d or 37 percent of the total water withdrawn by public-supply systems statewide. Of that amount, 79 percent, or 208 Mgalld, was used in western Tennessee.

Tennessee

Divide and conquer: Separating the two probabilities in seismic phase picking

There are two fundamental probabilities in the seismic phase picking process – the probability of the existence of a seismic phase (detection probability) and the probability of correctly identifying the phase arrival time (timing probability). The nearly ubiquitous approach in developing deep learning phase picking models is to use a kernel, such as a truncated Gaussian, to mask the labeled phase arrival time, and train a segmentation model. Once a model is trained, the times of the peaks in the output are taken as phase arrival times (picks) and the height of the peaks are taken as “probability” of the picks. Here, we show that this “probability” represents neither the detection nor the timing probabilty because this approach forces the output to follow the shape of the kernel. We introduce an approach using two models to estimate these two distinct probabilities. We use a binary classifier with a calibrated confidence to address the detection probability and a multi-class classifier to obtain a probability mass function to address the timing probability. This new approach makes the deep learning-based phase picking process more interpretable and gives us options to logically control seismic monitoring workflows.

Geophysical Journal International

Surface variable‐based machine learning for scalable arsenic prediction in undersampled areas

In the United States, private wells are not federally regulated, and many households do not test for Arsenic (As). Chronic exposure is linked with multiple health outcomes, and risk can change sharply over short distances and with well depth. Coarse maps or sparse sampling often miss exceedances. Most existing models operate at ∼1 km resolution and use groundwater chemistry or detailed geologic logs, which limits their use in undersampled areas where improved guidance is most needed. We overcome these limitations by developing a machine learning model for Minnesota, USA, that predicts As exposure risk using only surficial variables from remote sensing and global data sets. Variables related to surface water hydrology and geomorphology are selected based on mechanistic links that control redox conditions and As mobilization. Local training was essential, and surficial geology variables that are more sensitive to local conditions were needed to maximize model accuracy. The resulting complete model was sufficiently sensitive to generate accurate and detailed risk maps and depth profiles of As concentrations above the 10 μg/L maximum contaminant level. Accuracy depended on local training data density. We identified a training data density of 0.07 wells/km 2 as a practical target for stable county-level performance. Maps of exceedance probabilities highlight priority areas for testing that are particularly important in rural communities that have received less sampling. These results support public health action by guiding where to install wells and where to test them, how much new sampling is needed, and where treatment outreach is most urgent.

Minnesota

Season and antecedent conditions impact concentration-discharge relationships for dissolved organic carbon and alkalinity in southeast Alaskan watershed

Fluvial export of dissolved carbon plays an important role in watershed-scale biogeochemistry. Predicted changes in climate are expected to impact watershed hydrologic regimes, and in turn, the sources and export of dissolved carbon from watersheds. Here, we utilize high resolution measurements of discharge and dissolved carbon concentration to examine how concentration-discharge (CQ) relationships vary seasonally and during high flow events over the main runoff season (May–October) in a temperate forested watershed in Southeast Alaska. Concentration-discharge relationships for dissolved organic carbon (DOC) and alkalinity demonstrated strong seasonal patterns, with more linear relationships in May and June versus other months. Changing power law model slopes ( b values; the exponent in a power law regression between runoff and carbon yields) indicated potentially shifting watershed sources (biogenic vs. geologic) and contrasting dominant flowpaths (shallow vs. deeper groundwater) for DOC and alkalinity over the sampling period. During the largest storm event of the study, DOC and alkalinity b values shifted from an overall pattern of transport (mean b = 1.58 values >1.0 indicate transport limitation) and source limitation (mean b = 0.48, values <1.0 indicate source limitation) to chemostatic (DOC, b = 0.99; alkalinity, b = 1.019). In June through August, patterns in hysteresis index suggest that CQ relationships were altered when storms followed in close succession to each other. Together, these findings indicate that seasonal and antecedent flow conditions play a role in dissolved carbon export from forested watersheds. Understanding these dynamics, particularly during winter months, will become increasingly important as changes to hydroclimate impact riverine carbon export.

Alaska

Invasion of perennial sagebrush steppe by shallow-rooted exotic cheatgrass reduces stable forms of soil carbon in a warmer but not cooler ecoregion

Soil organic carbon ('SOC') in drylands comprises nearly a third of the global SOC pool and has relatively rapid turnover and thus is a key driver of variability in the global carbon cycle. SOC is also a sensitive indicator of longer-term directional change and disturbance-responses of ecosystem C storage. Biome-scale disruption of the dryland carbon cycle by exotic annual grass invasions (mainly Bromus tectorum, 'Cheatgrass') threatens carbon storage and corresponding benefits to soil hydrology and nutrient retention. Past studies on cheatgrass impacts mainly focused on total C, and of the few that evaluated SOC, none compared the very different fractions of SOC, such as relatively unstable particulate organic carbon (POC) or relatively stable, mineral-associated organic carbon (MAOC). We measured SOC and its POC and MAOC constituents in the surface soils of sites that had sagebrush canopies but differed in whether their understories had been invaded by cheatgrass or not, in both warm and relatively colder ecoregions of the western USA. MAOC stocks were 36.1% less in the 0–10 cm depth and 46.1% less in the 10–20 cm depth in the cheatgrass-invaded stands compared to the uninvaded stands of the warmer Colorado Plateau, but not in the cooler and more carbon-rich Wyoming Basin ecoregion. In plots where cheatgrass increased SOC, it was via unstable POC. These findings indicate that cheatgrass effects on the distribution of soil carbon among POC and MAOC fractions may vary among ecoregions, and that cheatgrass can reduce forms of carbon that are otherwise considered stable and 'secure', i.e. sequestered.

Environmental Research Communications

Hydrogeology, karst, and groundwater availability of Monroe County, West Virginia

Monroe County is in southeastern West Virginia, encompassing an area of 474 square miles. The area consists of karst and siliciclastic aquifers of Ordovician, Silurian, Devonian, and Mississippian age and is in parts of two physiographic provinces: the Valley and Ridge Province to the east of Peters Mountain, and the Appalachian Plateau Province to the west of Peters Mountain. This study was developed in response to inquiries from the Monroe County Commission requesting assessment of the water resources of the county to better understand the quantity of the county’s groundwater resources, for both current [2023] and future demand, and to provide information to support protection and management of the county’s valuable groundwater resources. Various products were developed for this study that provide knowledge with respect to water availability and contamination susceptibility of the karst aquifers within the county. U.S. Geological Survey (USGS) geologists conducted extensive geologic mapping in support of the project, producing (1) a countywide bedrock geologic map, (2) a countywide hydrogeologic map, and (3) a light detection and ranging (lidar)-derived countywide digital elevation model and associated sinkhole map. A significant part of this work was to map in detail the Greenbrier Group at the formation level, which prior to this study had only partially been completed. The report also includes (4) a description of the lithologic units identified as part of the geologic mapping process. U.S. Geological Survey hydrologists completed several additional products for the hydrology part of the effort, including development of (1) a countywide potentiometric surface (water-table) map, (2) a countywide base-flow stream assessment, (3) countywide water-budget estimates, (4) well log surveys for 15 wells to better understand subsurface controls on groundwater flow within the study area, (5) two groundwater tracer tests to better refine the groundwater divide from the northern and southern parts of the karst aquifer in Monroe County; and finally, based on all available data collected for the study including the potentiometric surface map, geologic map, current [2023] and legacy fluorometric groundwater tracer tests, and base-flow stream assessments, (6) groundwater-basin delineations were reassessed for principal groundwater basins within the Greenbrier aquifer. In Monroe County, four principal hydrogeologic settings produce large yields of water for residential, agricultural, and other uses. The most relied upon water-bearing zone with respect to current [2023] public water supply is from springs along Peters Mountain. These springs are derived from intervals of fractured sandstone and resultant alluvial deposits. Groundwater flows downslope through these permeable alluvial deposits and discharges at the contact with less permeable strata, such as the Reedsville Shale. The second most relied upon water-bearing zone in Monroe County is within the karstic Greenbrier Group aquifer, in which the basal Hillsdale Limestone overlies the less permeable Maccrady Shale. This geologic contact between the Hillsdale Limestone and Maccrady Shale is not only targeted as a source of water for agricultural supply but also is targeted as a source of water for residential supply. The third most relied upon water-bearing zone is composed of shallow perched aquifers within the Greenbrier Group. The discontinuous nature of these perched aquifers makes mapping their extent impossible, but they are related to permeable geologic strata, such as karstified limestones with solutionally enhanced permeability that overlies less permeable shale or chert bedrock. During geologic mapping of the county, several of these perched aquifers were documented in the Pickaway, Union, and Alderson Limestones. A fourth zone consists of springs from Ordovician carbonates at the base of Peters Mountain, which are influenced by sinking streams as well as upwelling along faults. In terms of water quantity, the most sustainable springs are those having deeper-sourced flows. Public supplies are a principal source of water used for residential and commercial supply in the region, accounting for 0.49 million gallons per day (Mgal/d) of fresh-water withdrawals (0.14 Mgal/d of groundwater and 0.35 Mgal/d of surface water) for residential and commercial use and serving 6,645 individuals (49.2 percent of the population). An estimated 6,861 people, (50.8 percent of the population) primarily rely on private wells or other unregulated sources, such as springs, and withdraw 0.55 Mgal/d of groundwater for their residential use. Public water supply in the region is primarily (71.4 percent) derived from springs and augmented by stream withdrawals (backup sources mainly during low-flow periods), with the remaining portion (28.6 percent) derived from groundwater withdrawals from wells. For rural residents, however, 100 percent of their withdrawals are derived from groundwater (wells or springs).

West Virginia

Mapping bedrock outcrops in the Sierra Nevada Mountains (California, USA) using machine learning

Accurate, high-resolution maps of bedrock outcrops can be valuable for applications such as models of land–atmosphere interactions, mineral assessments, ecosystem mapping, and hazard mapping. The increasing availability of high-resolution imagery can be coupled with machine learning techniques to improve regional bedrock outcrop maps. In the United States, the existing 30 m U.S. Geological Survey (USGS) National Land Cover Database (NLCD) tends to misestimate extents of barren land, which includes bedrock outcrops. This impacts many calculations beyond bedrock mapping, including soil carbon storage, hydrologic modeling, and erosion susceptibility. Here, we tested if a machine learning (ML) model could more accurately map exposed bedrock than NLCD across the entire Sierra Nevada Mountains (California, USA). The ML model was trained to identify pixels that are likely bedrock from 0.6 m imagery from the National Agriculture Imagery Program (NAIP). First, we labeled exposed bedrock at twenty sites covering more than 83 km 2 (0.13%) of the Sierra Nevada region. These labels were then used to train and test the model, which gave 83% precision and 78% recall, with a 90% overall accuracy of correctly predicting bedrock. We used the trained model to map bedrock outcrops across the entire Sierra Nevada region and compared the ML map with the NLCD map. At the twenty labeled sites, we found the NLCD barren land class, even though it includes more than just bedrock outcrops, accounted for only 41% and 40% of mapped bedrock from our labels and ML predictions, respectively. This substantial difference illustrates that ML bedrock models can have a role in improving land-cover maps, like NLCD, for a range of science applications.

California

Landsliding follows signatures of wildfire history and vegetative regrowth in a steep coastal shrubland

Five years after the deadly and destructive 9 January 2018 Montecito debris flows (Santa Barbara County, California, USA), an atmospheric river storm on 9 January 2023 triggered widespread landsliding that affected many of the same drainages in the Santa Ynez Mountains. Using high-resolution aerial imagery, we identified >10,000 landslides over an ∼160 km 2 area. Most of the landslides were shallow (<1 m in depth) translational debris slides that initiated on steep (∼40°), south-facing hillslopes, with the highest incidence of landsliding in a sandstone-dominated bedrock unit. The landslides mobilized into debris flows and delivered substantial quantities of sediment downstream, which contributed to costly infrastructure impairments. We detected order-of-magnitude differences in landslide density across the study area that could not be attributed to variations in geomorphology (topographic aspect and slope), geology (bedrock type), or hydrology (seasonal antecedent rainfall, peak hourly storm rainfall intensity, total storm rainfall), which are usually considered relevant factors for shallow landsliding. Rather, we found that vegetation regrowth following wildfire was likely a relevant factor associated with the highly variable landslide densities. Hillslopes with less and different types of vegetation regrowth after fire appear to have been more susceptible to shallow landslides. We identify a possible vegetation control on postfire landsliding, which highlights an opportunity for hypothesis testing using more advanced techniques to track the evolution of vegetation cover and vegetation type in steep shrubland environments following wildfire.

California

Microplastics undergo fragmentation during pressurized membrane filtration

Low-micrometer microplastics (<10 μm) have been detected in drinking water, driving growing interest in using pressure-driven membrane filtration to remove these particles and ensure drinking water safety. However, little attention is paid to the fate of microplastics concentrated in the filtration byproduct. In this study, using well-defined polystyrene (PS) and poly(methyl methacrylate) microspheres as model particles, we observed microplastic fragmentation during nanofiltration and the subsequent release of smaller fragments. After operating for 3 h at 20 bar, 67.9 ± 8.0% of the PS spheres in the concentrate, based on particles counted in selected fields of view, were transformed into fractured particles. The characteristic Raman band signals of microplastics were significantly weakened after fragmentation, leading to detection challenges. To address this, a data processing algorithm was developed to identify PS fragments as small as 1 μm. Preliminary statistical analysis reveals that within the tested pressure range, operation time has a stronger influence on fragmentation than pressure magnitude alone and that fragmentation is further governed by the intrinsic mechanical properties of the tested model polymers. This work provides direct evidence that pressure-driven membrane processes induce microplastic fragmentation and highlights the environmental risks associated with the discharge of fragmented microplastics into the concentrate.

Environmental Science & Technology Letters

Rock sample photogrammetry

This step-by-step protocol describes the photogrammetry process used by the U.S. Geological Survey Spokane Imaging Lab (SPIMG) lab to create 3D models of geologic samples. Steps related to photographing small objects are applicable to photogrammetry in general, however, SPIMG-specific steps involving lab hardware and software may not be.

Protocols.io