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Phoebe L. Hauff

Publications and source records attributed to Phoebe L. Hauff.

8 recordsLinked to original sources

The handling, hazards, and maintenance of heavy liquids in the geologic laboratory

In geologic laboratories the organic heavy liquids bromoform, methylene iodide, tetrabromoethane, and clerici compounds have been used for years in mineral separation processes. Because the volume of use of these compounds is low, insufficient data is available on their toxic properties. This report is an attempt to summarize the known data from published and industry sources. The physical properties, hazards of handling,proper storage facilities, and adequate protective Clothing are discussed for each compound as well as for their common and less-common solvents. Toxicity data for these materials is listed along with exposure symptoms and suggested first aid treatments. Safety for the worker is emphasized. Three reclamation methods which recover the solvent used as a dilutant and purify the heavy liquid are discussed and illustrated. These include: the water cascade, re fluxing-distillation-condensation, and flash evaporation methods. Various techniques for restoration and stabilization of these heavy liquids are also included.

Circular↗

Least-squares refinement of powder diffraction data for unit cell parameters: Program listing for DEC 10 computer

This FORTRAN computer program is a time-sharing version of the classic program of Appleman and Evans (1973) and Evans, Appleman, and Handwerker (1963), which indexes powder patterns and refines unit-cell dimensions. The program, originally written to be processed in batch mode for an IBM computer, was modified to run in time-sharing mode on the DEC 10 computer. This version does not depart philosophically from the original program; however, the input and output formats have been adapted to the time-sharing terminal. These modifications and the actual running of the program are not discussed in detail here, as this report is intended only to make the program itself available. Examples of the input and output formats are shown on pages 3-8. Input can be entered through the terminal by two methods. An input file may either be independently created and then entered into the program later, or created directly through the interactive mode of the program. With the latter method a file of the input information may also be saved for later use. Both methods allow for the data to be edited after each refinement run. The output format has been changed to an 80-column width, common to many terminals. Only the last refinement cycle is printed and some of the statistical computations have been surpressed. Using the "Unit Cell" program from the terminal in a "real time" situation emphasizes the versatility of the program. This ability to interact directly with the computer gives the user a better appreciation of the program, its options, the data, and the problem being solved.

Open-File Report↗

Laboratory manual: mineral X-ray diffraction data retrieval/plot computer program

The Mineral X-Ray Diffraction Data Retrieval/Plot Computer Program--XRDPLT (VanTrump and Hauff, 1976a) is used to retrieve and plot mineral X-ray diffraction data. The program operates on a file of mineral powder diffraction data (VanTrump and Hauff, 1976b) which contains two-theta or 'd' values, and intensities, chemical formula, mineral name, identification number, and mineral group code. XRDPLT is a machine-independent Fortran program which operates in time-sharing mode on a DEC System i0 computer and the Gerber plotter (Evenden, 1974). The program prompts the user to respond from a time-sharing terminal in a conversational format with the required input information. The program offers two major options: retrieval only; retrieval and plot. The first option retrieves mineral names, formulas, and groups from the file by identification number, by the mineral group code (a classification by chemistry or structure), or by searches based on the formula components. For example, it enables the user to search for minerals by major groups (i.e., feldspars, micas, amphiboles, oxides, phosphates, carbonates) by elemental composition (i.e., Fe, Cu, AI, Zn), or by a combination of these (i.e., all copper-bearing arsenates). The second option retrieves as the first, but also plots the retrieved 2-theta and intensity values as diagrammatic X-ray powder patterns on mylar sheets or overlays. These plots can be made using scale combinations compatible with chart recorder diffractograms and 114.59 mm powder camera films. The overlays are then used to separate or sieve out unrelated minerals until unknowns are matched and identified.

Open-File Report↗