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Irving May

Publications and source records attributed to Irving May.

13 recordsLinked to original sources

Determination of beryllium in ores and rocks by a dilution-fluorometric method with morin

Beryllium in concentrations as little as a few parts per million is determined fluorometrically with morin in low grade ores by a dilution method without separations. A high sensitivity is obtained by the adoption of instrumental and reaction conditions that give a satisfactory ratio of beryllium to blank fluorescence and at the same time minimize iron interference. Data on the behavior of 47 ions are given. The method is applied to ores containing bertrandite and beryl as the beryllium minerals.

Analytical Chemistry

An improved fluorimeter for the determination of uranium in fluoride melts

The Model R fluorimeter has been modified to increase its stability and sensitivity. The new instrument* is about ten times as sensitive as the original fluorimeter, but it can also be employed conveniently at a sensitivity level comparable to or less than that of the Model R fluorimeter. *The modified fluorimeter described here was developed in the latter half of 1948 and has since been in constant use in the laboratory for routine analysis. Although it is now being superseded to a large extent by a more recently developed transmission fluorimeter, the modified fluorimeter is a very useful tool for many types of analysis. (Fletcher, M. H., May, Irving, and Slavin, Morris, A transmission fluorimeter for use in the fluorimetric method of analysis for uranium: Trace Elements Investigations Report 104, August 1949.)

Trace Elements Investigations

The design of the Model V transmission fluorimeter

The transmission fluorimeter for the measurement of the fluorescence of uranium in fluoride melts is described. The instrument incorporates several improved features which have not been published previously. Unlike the earliest models, the design of the new fluorimeter, with its close machining of parts, reduces the possibility of light leakage and also increases considerably the ease with which the various components of the instrument may be assembled and adjusted. The Model V fluorimeter is a very rugged instrument with a compact arrangement of parts. It possess great flexibility so that various phototubes, measuring devices, light sources, and filter combinations may be used interchangeably. Detailed shop drawings are given for the construction of the fluorimeter.

Trace Elements Investigations