Rapid field and laboratory method for the determination of copper in soil and rocks
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Geology topics
Publications and source records attributed to Hy Almond.
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The field methods described in this report are those currently used in geochemical prospecting by the U. S. Geological Survey. Some have been published, others are being processed for publication, while others are still being investigated. The purpose in compiling these methods is to make them readily available in convenient form. The methods have not been thoroughly tested and none is wholly satisfactory. Research is being continued.
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A method is described for the field estimation of total zinc in soils. A small sample of soil is fused with potassium bisulfate, the fused mass dissolved in water, buffered at pH 4 to 5.5 with acetate buffer, and sodium thiosulfate added to form complex ions with metals that might cause interference. Measured increments of the sample solution are added to a carbon-tetrachloride-dithizone solution, with vigorous shaking after each addition, until a standard color is obtained in the organic phase. Under favorable conditions up to 60 determinations per day can be made by one man. Comparisons of data obtained by the field method with accurate laboratory analyses of the same samples indicate that the method is sufficiently reliable for reconnaissance surveys.